3,4,5-trimethoxy-N-(((3-(4-methoxybenzoyl)aminophenyl)amino)carbonothioyl)benzamide

Base Information

Chemical Name:3,4,5-trimethoxy-N-(((3-(4-methoxybenzoyl)aminophenyl)amino)carbonothioyl)benzamide
CAS No.:1192927-80-2
Molecular Formula:C₂₅H₂₅N₃O₆S
Molecular Weight:495.556
Hs Code.:

Synonyms:3,4,5-trimethoxy-N-(((3-(4-methoxybenzoyl)aminophenyl)amino)carbonothioyl)benzamide

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Chemical Property of 3,4,5-trimethoxy-N-(((3-(4-methoxybenzoyl)aminophenyl)amino)carbonothioyl)benzamide

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Technology Process of 3,4,5-trimethoxy-N-(((3-(4-methoxybenzoyl)aminophenyl)amino)carbonothioyl)benzamide

There total 7 articles about 3,4,5-trimethoxy-N-(((3-(4-methoxybenzoyl)aminophenyl)amino)carbonothioyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1147550-11-5
ammonium thiocyanate

: 4521-61-3
3,4,5-Trimethoxybenzoyl chloride

: 41378-23-8
N-(3-amino-phenyl)-4-methoxy-benzamide

: 1192927-80-2
3,4,5-trimethoxy-N-(((3-(4-methoxybenzoyl)aminophenyl)amino)carbonothioyl)benzamide

Guidance literature:: ammonium thiocyanate; 3,4,5-Trimethoxybenzoyl chloride; In acetone; for 0.333333h; Reflux;

N-(3-amino-phenyl)-4-methoxy-benzamide; In acetone; for 1h; Reflux;

Reference yield:

: 96748-36-6
4-methoxy-N-(3-nitrophenyl)benzamide

: 1192927-80-2
3,4,5-trimethoxy-N-(((3-(4-methoxybenzoyl)aminophenyl)amino)carbonothioyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonium formate / palladium on activated charcoal / methanol / 0.07 h / 80 °C / Microwave irradiation

2.1: acetone / 0.33 h / Reflux

2.2: 1 h / Reflux

With ammonium formate; palladium on activated charcoal; In methanol; acetone;

Reference yield:

: 100-07-2
4-methoxy-benzoyl chloride

: 1192927-80-2
3,4,5-trimethoxy-N-(((3-(4-methoxybenzoyl)aminophenyl)amino)carbonothioyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 2.5 h / 20 °C / Cooling with ice

2.1: ammonium formate / palladium on activated charcoal / methanol / 0.07 h / 80 °C / Microwave irradiation

3.1: acetone / 0.33 h / Reflux

3.2: 1 h / Reflux

With ammonium formate; triethylamine; palladium on activated charcoal; In methanol; dichloromethane; acetone;