1-(p-toluenesulfonyl)-2H,3H,4H,1aH,8bH-benzo[f]oxirane[2,3-d]azaperhydroepine

Base Information

Chemical Name:1-(p-toluenesulfonyl)-2H,3H,4H,1aH,8bH-benzo[f]oxirane[2,3-d]azaperhydroepine
CAS No.:585578-16-1
Molecular Formula:C₁₇H₁₇NO₃S
Molecular Weight:315.393
Hs Code.:

Synonyms:1-(p-toluenesulfonyl)-2H,3H,4H,1aH,8bH-benzo[f]oxirane[2,3-d]azaperhydroepine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(p-toluenesulfonyl)-2H,3H,4H,1aH,8bH-benzo[f]oxirane[2,3-d]azaperhydroepine

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Technology Process of 1-(p-toluenesulfonyl)-2H,3H,4H,1aH,8bH-benzo[f]oxirane[2,3-d]azaperhydroepine

There total 1 articles about 1-(p-toluenesulfonyl)-2H,3H,4H,1aH,8bH-benzo[f]oxirane[2,3-d]azaperhydroepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20426-63-5
1-(p-Tolylsulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine

: 585578-16-1
1-(p-toluenesulfonyl)-2H,3H,4H,1aH,8bH-benzo[f]oxirane[2,3-d]azaperhydroepine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃; for 5h;

Reference yield:

: 585578-16-1
1-(p-toluenesulfonyl)-2H,3H,4H,1aH,8bH-benzo[f]oxirane[2,3-d]azaperhydroepine

: 4-hydroxy-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

Reference yield:

: 585578-16-1
1-(p-toluenesulfonyl)-2H,3H,4H,1aH,8bH-benzo[f]oxirane[2,3-d]azaperhydroepine

: 4-oxo-1-(p-toluenesulfonyl)-2,3,4,5-tetrahydro-1H-1-benzazepine

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 - 20 °C

2: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

With lithium aluminium tetrahydride; sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane;