Dithiophosphoric acid S-[1,3-bis-(4-methoxy-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester

Base Information

Chemical Name:Dithiophosphoric acid S-[1,3-bis-(4-methoxy-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester
CAS No.:79359-75-4
Molecular Formula:C₂₁H₂₇O₅PS₂
Molecular Weight:454.548
Hs Code.:

Synonyms:Dithiophosphoric acid S-[1,3-bis-(4-methoxy-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dithiophosphoric acid S-[1,3-bis-(4-methoxy-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester

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Technology Process of Dithiophosphoric acid S-[1,3-bis-(4-methoxy-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester

There total 1 articles about Dithiophosphoric acid S-[1,3-bis-(4-methoxy-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2373-89-9
4,4'-dimethoxychalcone

: 298-06-6
O,O-Diethyl hydrogen phosphorodithioate

: 79359-75-4
Dithiophosphoric acid S-[1,3-bis-(4-methoxy-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester

Guidance literature:: In benzene; at 50 - 60 ℃; for 3h;
DOI:10.1055/s-1981-29521

Reference yield:

: 79359-75-4
Dithiophosphoric acid S-[1,3-bis-(4-methoxy-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester

: 345207-88-7
2,4-Bis-(4-methoxy-phenyl)-thietane

Guidance literature:: With sodium tetrahydroborate; sodium hydride; Yield given. Multistep reaction; t-butanol 1.) room temp., 3 h, 2.) 60 deg C, 1 h, 3.) room temp., 4 h, 4.) 60 deg C, 1 h;
DOI:10.1055/s-1981-29521