5-Isopropyl-1-[3-(3-methyl-2-nitro-phenoxy)-propyl]-4-phenyl-1H-imidazole

Base Information

Chemical Name:5-Isopropyl-1-[3-(3-methyl-2-nitro-phenoxy)-propyl]-4-phenyl-1H-imidazole
CAS No.:1027578-90-0
Molecular Formula:C₂₂H₂₅N₃O₃
Molecular Weight:379.459
Hs Code.:

Synonyms:5-Isopropyl-1-[3-(3-methyl-2-nitro-phenoxy)-propyl]-4-phenyl-1H-imidazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Isopropyl-1-[3-(3-methyl-2-nitro-phenoxy)-propyl]-4-phenyl-1H-imidazole

Chemical Property:

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Technology Process of 5-Isopropyl-1-[3-(3-methyl-2-nitro-phenoxy)-propyl]-4-phenyl-1H-imidazole

There total 6 articles about 5-Isopropyl-1-[3-(3-methyl-2-nitro-phenoxy)-propyl]-4-phenyl-1H-imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1025901-58-9
N-(1-Benzoyl-2-methyl-propyl)-N-[3-(3-methyl-2-nitro-phenoxy)-propyl]-formamide

: 1027578-90-0
5-Isopropyl-1-[3-(3-methyl-2-nitro-phenoxy)-propyl]-4-phenyl-1H-imidazole

Guidance literature:: With formic acid; ammonium formate; formamide; at 120 ℃; for 2h;
DOI:10.1021/jm00063a014

Reference yield:

: 4920-77-8
3-methyl-2-nitrophenol

: 1027578-90-0
5-Isopropyl-1-[3-(3-methyl-2-nitro-phenoxy)-propyl]-4-phenyl-1H-imidazole

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / K₂CO₃ / dimethylformamide / 2 h / 60 °C

2: 90 percent / NaI / dimethylformamide / 1 h / 100 °C

3: 86 percent / KOH / ethanol / 0.17 h / Ambient temperature

4: 1.) NaH / 1.) DMF, 60 deg C, 1 h, 2.) DMF, 1 h

5: ammonium formate, formic acid, formamide / 2 h / 120 °C

With potassium hydroxide; formic acid; ammonium formate; sodium hydride; potassium carbonate; formamide; sodium iodide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00063a014

Reference yield:

: 141816-23-1
3-(3-chloropropoxy)-2-nitrotoluene

: 1027578-90-0
5-Isopropyl-1-[3-(3-methyl-2-nitro-phenoxy)-propyl]-4-phenyl-1H-imidazole

Guidance literature:: Multi-step reaction with 4 steps

1: 90 percent / NaI / dimethylformamide / 1 h / 100 °C

2: 86 percent / KOH / ethanol / 0.17 h / Ambient temperature

3: 1.) NaH / 1.) DMF, 60 deg C, 1 h, 2.) DMF, 1 h

4: ammonium formate, formic acid, formamide / 2 h / 120 °C

With potassium hydroxide; formic acid; ammonium formate; sodium hydride; formamide; sodium iodide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00063a014