3-[2-(3-Methyl-thioureido)-ethylsulfanylmethyl]-2H-pyridine-1-carboxylic acid phenyl ester

Base Information

Chemical Name:3-[2-(3-Methyl-thioureido)-ethylsulfanylmethyl]-2H-pyridine-1-carboxylic acid phenyl ester
CAS No.:102564-84-1
Molecular Formula:C₁₇H₂₁N₃O₂S₂
Molecular Weight:363.505
Hs Code.:

Synonyms:3-[2-(3-Methyl-thioureido)-ethylsulfanylmethyl]-2H-pyridine-1-carboxylic acid phenyl ester

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Chemical Property of 3-[2-(3-Methyl-thioureido)-ethylsulfanylmethyl]-2H-pyridine-1-carboxylic acid phenyl ester

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Technology Process of 3-[2-(3-Methyl-thioureido)-ethylsulfanylmethyl]-2H-pyridine-1-carboxylic acid phenyl ester

There total 3 articles about 3-[2-(3-Methyl-thioureido)-ethylsulfanylmethyl]-2H-pyridine-1-carboxylic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 38603-42-8
N-methyl-N¹-<2-(3-pyridinylmethylthio)ethyl>thiourea

: 1885-14-9
phenyl chloroformate

: 102564-84-1
3-[2-(3-Methyl-thioureido)-ethylsulfanylmethyl]-2H-pyridine-1-carboxylic acid phenyl ester

Guidance literature:: With sodium tetrahydroborate; In methanol; diethyl ether; at -69 ℃; for 3h;

Reference yield:

: 52761-08-7
3-pyridinemethanol hydrochloride

: 102564-84-1
3-[2-(3-Methyl-thioureido)-ethylsulfanylmethyl]-2H-pyridine-1-carboxylic acid phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / 48 percent HBr / 18 h / Heating

2: 1.) K₂CO₃ / 1.) water; 2.) isopropanol, 1.5 h, reflux

3: 70 percent / NaBH₄ / methanol; diethyl ether / 3 h / -69 °C

With sodium tetrahydroborate; hydrogen bromide; potassium carbonate; In methanol; diethyl ether;

Reference yield:

: 38585-40-9
2-<(3-aminoethyl)thiomethyl>pyridine dihydrobromide

: 102564-84-1
3-[2-(3-Methyl-thioureido)-ethylsulfanylmethyl]-2H-pyridine-1-carboxylic acid phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) K₂CO₃ / 1.) water; 2.) isopropanol, 1.5 h, reflux

2: 70 percent / NaBH₄ / methanol; diethyl ether / 3 h / -69 °C

With sodium tetrahydroborate; potassium carbonate; In methanol; diethyl ether;