Technology Process of 2-phenyl-1,3-propanedithiol
There total 9 articles about 2-phenyl-1,3-propanedithiol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-Phenyl-1,3-propandiol-di-p-toluolsulfonsaeureester;
With
thiourea;
In
ethanol;
Inert atmosphere;
Reflux;
With
sodium hydroxide;
In
ethanol;
Reflux;
DOI:10.1016/j.tet.2013.08.061
- Guidance literature:
-
2-phenylpropane-1,3-diyl dimethanesulfonate;
With
thiourea;
In
isopropyl alcohol;
for 24h;
Reflux;
Inert atmosphere;
With
sodium hydroxide;
In
water; isopropyl alcohol;
for 24h;
Reflux;
Inert atmosphere;
With
methanol; sodium tetrahydroborate;
In
tetrahydrofuran;
at 0 ℃;
for 2h;
DOI:10.1021/ol302244f
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine / dichloromethane / 0 °C / Inert atmosphere
2.1: thiourea / isopropyl alcohol / 24 h / Reflux; Inert atmosphere
2.2: 24 h / Reflux; Inert atmosphere
2.3: 2 h / 0 °C
With
triethylamine; thiourea;
In
dichloromethane; isopropyl alcohol;
DOI:10.1021/ol302244f
