(4-{[Bis-(2-tert-butoxycarbonylamino-ethylamino)-methylene]-sulfamoyl}-phenoxy)-acetic acid

Base Information

Chemical Name:(4-{[Bis-(2-tert-butoxycarbonylamino-ethylamino)-methylene]-sulfamoyl}-phenoxy)-acetic acid
CAS No.:181780-05-2
Molecular Formula:C₂₃H₃₇N₅O₉S
Molecular Weight:559.641
Hs Code.:

Synonyms:(4-{[Bis-(2-tert-butoxycarbonylamino-ethylamino)-methylene]-sulfamoyl}-phenoxy)-acetic acid

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Chemical Property of (4-{[Bis-(2-tert-butoxycarbonylamino-ethylamino)-methylene]-sulfamoyl}-phenoxy)-acetic acid

Chemical Property:

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Technology Process of (4-{[Bis-(2-tert-butoxycarbonylamino-ethylamino)-methylene]-sulfamoyl}-phenoxy)-acetic acid

There total 11 articles about (4-{[Bis-(2-tert-butoxycarbonylamino-ethylamino)-methylene]-sulfamoyl}-phenoxy)-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 181780-02-9
(4-{[Bis-(2-tert-butoxycarbonylamino-ethylamino)-methylene]-sulfamoyl}-phenoxy)-acetic acid ethyl ester

: 181780-05-2
(4-{[Bis-(2-tert-butoxycarbonylamino-ethylamino)-methylene]-sulfamoyl}-phenoxy)-acetic acid

Guidance literature:: With lithium hydroxide; In 1,4-dioxane; water; Ambient temperature;
DOI:10.1016/0040-4039(96)01058-1

Reference yield:

: 98-67-9
p-hydoroxybenzenesulfonic acid

: 181780-05-2
(4-{[Bis-(2-tert-butoxycarbonylamino-ethylamino)-methylene]-sulfamoyl}-phenoxy)-acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / dimethylformamide / Ambient temperature

2: SOCl₂ / toluene / 100 °C

3: 17 percent / NaOH / acetone / Ambient temperature; pH 10

4: 92 percent / LiOH / H₂O; dioxane / Ambient temperature

With lithium hydroxide; sodium hydroxide; thionyl chloride; potassium carbonate; In 1,4-dioxane; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/0040-4039(96)01058-1

Reference yield:

: 57260-73-8
N-BOC-1,2-diaminoethane

: 181780-05-2
(4-{[Bis-(2-tert-butoxycarbonylamino-ethylamino)-methylene]-sulfamoyl}-phenoxy)-acetic acid

Guidance literature:: Multi-step reaction with 6 steps

1: K₂CO₃ / CHCl₃; H₂O / Heating

2: ethanol

3: acetone / Ambient temperature

4: 99 percent / NH₃ / methanol / 70 °C

5: 17 percent / NaOH / acetone / Ambient temperature; pH 10

6: 92 percent / LiOH / H₂O; dioxane / Ambient temperature

With lithium hydroxide; sodium hydroxide; ammonia; potassium carbonate; In 1,4-dioxane; methanol; ethanol; chloroform; water; acetone;
DOI:10.1016/0040-4039(96)01058-1