1,3-bis(2-trifluoromethyl-4-aminophenoxy)-5-(2,3,5,6-tetrafluoro-4-vinylphenoxy)benzene

Base Information

Chemical Name:1,3-bis(2-trifluoromethyl-4-aminophenoxy)-5-(2,3,5,6-tetrafluoro-4-vinylphenoxy)benzene
CAS No.:1396314-59-2
Molecular Formula:C₂₈H₁₆F₁₀N₂O₃
Molecular Weight:618.431
Hs Code.:

Synonyms:1,3-bis(2-trifluoromethyl-4-aminophenoxy)-5-(2,3,5,6-tetrafluoro-4-vinylphenoxy)benzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3-bis(2-trifluoromethyl-4-aminophenoxy)-5-(2,3,5,6-tetrafluoro-4-vinylphenoxy)benzene

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Technology Process of 1,3-bis(2-trifluoromethyl-4-aminophenoxy)-5-(2,3,5,6-tetrafluoro-4-vinylphenoxy)benzene

There total 2 articles about 1,3-bis(2-trifluoromethyl-4-aminophenoxy)-5-(2,3,5,6-tetrafluoro-4-vinylphenoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 653-34-9,26838-55-1
2,3,4,5,6-pentafluorostyrene

: 1396314-56-9
3,5-bis(4-amino-2-trifluoromethylphenoxy)phenol

: 1396314-59-2
1,3-bis(2-trifluoromethyl-4-aminophenoxy)-5-(2,3,5,6-tetrafluoro-4-vinylphenoxy)benzene

Guidance literature:: With calcium hydride; cesium fluoride; In N,N-dimethyl acetamide; at 80 ℃; for 18h; Inert atmosphere; Darkness;
DOI:10.1002/pola.27007

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 777-37-7
4-chloro-3-(trifluoromethyl)nitrobenzene

: 1396314-59-2
1,3-bis(2-trifluoromethyl-4-aminophenoxy)-5-(2,3,5,6-tetrafluoro-4-vinylphenoxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide; toluene / 5 h / 120 °C / Dean-Stark; Inert atmosphere

2: calcium hydride; cesium fluoride / N,N-dimethyl acetamide / 18 h / 80 °C / Inert atmosphere; Darkness

With calcium hydride; potassium carbonate; cesium fluoride; In N,N-dimethyl acetamide; N,N-dimethyl-formamide; toluene;
DOI:10.1002/pola.27007