PhSO₂CH₂CH₂CH₂OCPh₃

Base Information

Chemical Name:PhSO₂CH₂CH₂CH₂OCPh₃
CAS No.:1190600-23-7
Molecular Formula:C₂₈H₂₆O₃S
Molecular Weight:442.579
Hs Code.:

PhSO<sub>2</sub>CH<sub>2</sub>CH<sub>2</sub>CH<sub>2</sub>OCPh<sub>3</sub>

Synonyms:PhSO₂CH₂CH₂CH₂OCPh₃

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Chemical Property of PhSO₂CH₂CH₂CH₂OCPh₃

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Technology Process of PhSO₂CH₂CH₂CH₂OCPh₃

There total 1 articles about PhSO₂CH₂CH₂CH₂OCPh₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 25062-90-2
3-phenylsulfonylpropanol

: 76-83-5
trityl chloride

: 1190600-23-7
PhSO₂CH₂CH₂CH₂OCPh₃

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 48h;
DOI:10.1016/j.jorganchem.2009.05.035

Reference yield: 78.0%

: 1190600-23-7
PhSO₂CH₂CH₂CH₂OCPh₃

: Li[CH(SO₂Ph)CH₂CH₂OCPh₃]

Guidance literature:: With n-butyllithium; In hexane; toluene; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.jorganchem.2009.05.035

Reference yield: 42.0%

: 1190600-23-7
PhSO₂CH₂CH₂CH₂OCPh₃

: 1461-22-9
tributyltin chloride

: 1190600-29-3
PhSO₂CH(Sn(n-Bu)3)CH₂CH₂OCPh₃

Guidance literature:: With n-butyllithium; In pentane; Schlenk technique, under Ar; to nBuLi in pentane, sulfone deriv. added, after 24 h Sn(n-Bu)3 added slowly; water added, aq. phase extd. with Et2O; org. extracts dried, filtered, solvent evapd., purified by thin layer chromy. on silica, using pentane/Et2O; elem. anal.;
DOI:10.1016/j.jorganchem.2009.05.035