3-diethylcarbamoyl-5-methoxyphenyl trifluoromethanesulsonate

Base Information

• Chemical Name: 3-diethylcarbamoyl-5-methoxyphenyl trifluoromethanesulsonate
• CAS No.: 1025765-88-1
• Molecular Formula: C₁₃H₁₆F₃NO₅S
• Molecular Weight: 355.335
• Mol file: 1025765-88-1.mol

Synonyms:3-diethylcarbamoyl-5-methoxyphenyl trifluoromethanesulsonate

Chemical Property of 3-diethylcarbamoyl-5-methoxyphenyl trifluoromethanesulsonate

Chemical Property:

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Technology Process of 3-diethylcarbamoyl-5-methoxyphenyl trifluoromethanesulsonate

There total 1 articles about 3-diethylcarbamoyl-5-methoxyphenyl trifluoromethanesulsonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

N,N-diethyl 3-hydroxy-5-methoxybenzamide (908609-54-1) + N,N-phenylbistrifluoromethane-sulfonimide (37595-74-7) → 3-diethylcarbamoyl-5-methoxyphenyl trifluoromethanesulsonate (1025765-88-1)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1016/j.tet.2008.02.065

upstream raw materials:

N,N-diethyl 3-hydroxy-5-methoxybenzamide

N,N-phenylbistrifluoromethane-sulfonimide