ethyl (E)-4-[2-n-butyl-1-{(2-chlorophenyl)-methyl)-1H-imidazole-5-yl]-3-(5-methyl-furan-2-yl)methyl-3-butenoate

Base Information

Chemical Name:ethyl (E)-4-[2-n-butyl-1-{(2-chlorophenyl)-methyl)-1H-imidazole-5-yl]-3-(5-methyl-furan-2-yl)methyl-3-butenoate
CAS No.:1238973-22-2
Molecular Formula:C₂₆H₃₁ClN₂O₃
Molecular Weight:454.997
Hs Code.:

Synonyms:ethyl (E)-4-[2-n-butyl-1-{(2-chlorophenyl)-methyl)-1H-imidazole-5-yl]-3-(5-methyl-furan-2-yl)methyl-3-butenoate

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Chemical Property of ethyl (E)-4-[2-n-butyl-1-{(2-chlorophenyl)-methyl)-1H-imidazole-5-yl]-3-(5-methyl-furan-2-yl)methyl-3-butenoate

Chemical Property:

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Technology Process of ethyl (E)-4-[2-n-butyl-1-{(2-chlorophenyl)-methyl)-1H-imidazole-5-yl]-3-(5-methyl-furan-2-yl)methyl-3-butenoate

There total 7 articles about ethyl (E)-4-[2-n-butyl-1-{(2-chlorophenyl)-methyl)-1H-imidazole-5-yl]-3-(5-methyl-furan-2-yl)methyl-3-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ethyl (E)-3-[2-n-butyl-1-{(2-chlorophenyl)methyl}-1H-imidazol-5-yl]-2-(5-methyl-furan-2-yl)methyl-2-propenyl carbonate

: 1238973-22-2
ethyl (E)-4-[2-n-butyl-1-{(2-chlorophenyl)-methyl)-1H-imidazole-5-yl]-3-(5-methyl-furan-2-yl)methyl-3-butenoate

Guidance literature:: With triphenylphosphine; palladium diacetate; In tetrahydrofuran;

Reference yield:

: 17849-38-6
2-Chlorobenzyl alcohol

: 1238973-22-2
ethyl (E)-4-[2-n-butyl-1-{(2-chlorophenyl)-methyl)-1H-imidazole-5-yl]-3-(5-methyl-furan-2-yl)methyl-3-butenoate

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide; trifluoromethylsulfonic anhydride / methanol; dichloromethane

2: manganese dioxide / hexane; dichloromethane; toluene

4: diisobutylaluminium hydride; acetic acid / tetrahydrofuran; dichloromethane; toluene

5: hexane; dichloromethane; ethyl acetate

6: triphenylphosphine / palladium diacetate / tetrahydrofuran

With sodium hydroxide; manganese dioxide; trifluoromethylsulfonic anhydride; diisobutylaluminium hydride; acetic acid; triphenylphosphine; palladium diacetate; In tetrahydrofuran; methanol; hexane; dichloromethane; ethyl acetate; toluene;

Reference yield:

: 133485-55-9
2-n-butyl-1-(2-chlorophenyl)-methyl-5-hydroxymethyl-1H-imidazole

: 1238973-22-2
ethyl (E)-4-[2-n-butyl-1-{(2-chlorophenyl)-methyl)-1H-imidazole-5-yl]-3-(5-methyl-furan-2-yl)methyl-3-butenoate

Guidance literature:: Multi-step reaction with 5 steps

1: manganese dioxide / hexane; dichloromethane; toluene

3: diisobutylaluminium hydride; acetic acid / tetrahydrofuran; dichloromethane; toluene

4: hexane; dichloromethane; ethyl acetate

5: triphenylphosphine / palladium diacetate / tetrahydrofuran

With manganese dioxide; diisobutylaluminium hydride; acetic acid; triphenylphosphine; palladium diacetate; In tetrahydrofuran; hexane; dichloromethane; ethyl acetate; toluene;