C₅₆H₁₀₂O₉SSi₃

Base Information

• Chemical Name: C₅₆H₁₀₂O₉SSi₃
• CAS No.: 1028432-81-6
• Molecular Formula: C₅₆H₁₀₂O₉SSi₃
• Molecular Weight: 1035.74
• Mol file: 1028432-81-6.mol

Synonyms:C₅₆H₁₀₂O₉SSi₃

Chemical Property of C₅₆H₁₀₂O₉SSi₃

Chemical Property:

Purity/Quality:

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MSDS Files:

Useful:

Technology Process of C₅₆H₁₀₂O₉SSi₃

There total 4 articles about C₅₆H₁₀₂O₉SSi₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

C38H60O9S (1028433-12-6) + t-butyldimethylsiyl triflate (69739-34-0) → C56H102O9SSi3 (1028432-81-6)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 5.5h; Inert atmosphere;

DOI:10.1021/ol800685c

Reference yield:

C62H96O11Si2 (1360873-01-3) → C56H102O9SSi3 (1028432-81-6)

Guidance literature:

Multi-step reaction with 4 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

1.2: 0 - 20 °C

2.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

3.1: hydrogenchloride / tetrahydrofuran; methanol; water / 21.5 h / 60 °C

3.2: 20 h / 20 °C

4.1: triethylamine / dichloromethane / 9.17 h / 0 - 20 °C

With hydrogenchloride; tetrapropylammonium perruthennate; dimethylsulfide borane complex; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1002/chem.201101437

Reference yield:

C62H98O12Si2 (1360873-10-4) → C56H102O9SSi3 (1028432-81-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0 - 20 °C / Molecular sieve

2.1: hydrogenchloride / tetrahydrofuran; methanol; water / 21.5 h / 60 °C

2.2: 20 h / 20 °C

3.1: triethylamine / dichloromethane / 9.17 h / 0 - 20 °C

With hydrogenchloride; tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane; water;

DOI:10.1002/chem.201101437

upstream raw materials:

C₃₈H₆₀O₉S

t-butyldimethylsiyl triflate

C₆₂H₉₆O₁₁Si₂

C₆₂H₉₈O₁₂Si₂

Downstream raw materials:

C₅₅H₁₀₀O₉Si₃