C₂₂H₂₉N₅O₄*ClH

Base Information

Chemical Name:C₂₂H₂₉N₅O₄*ClH
CAS No.:1438021-20-5
Molecular Formula:C₂₂H₂₉N₅O₄*ClH
Molecular Weight:463.964
Hs Code.:

C<sub>22</sub>H<sub>29</sub>N<sub>5</sub>O<sub>4</sub>*ClH

Synonyms:C₂₂H₂₉N₅O₄*ClH

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₉N₅O₄*ClH

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Technology Process of C₂₂H₂₉N₅O₄*ClH

There total 8 articles about C₂₂H₂₉N₅O₄*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1438021-06-7
C₂₇H₃₇N₅O₆

: 1438021-20-5
C₂₂H₂₉N₅O₄*ClH

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 12h;
DOI:10.1021/ja4025148

Reference yield:

: 1438020-58-6
C₂₀H₂₃NO₆

: 1438021-20-5
C₂₂H₂₉N₅O₄*ClH

Guidance literature:: Multi-step reaction with 5 steps

1.1: palladium 10% on activated carbon; formic acid; hydrogen / methanol / 2 h

2.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h / 70 °C

2.2: 12 h / 20 °C

3.1: trifluoroacetic acid; hydrogenchloride / dichloromethane; water / 12 h / 20 °C

4.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; 4-methyl-morpholine / N,N-dimethyl-formamide / 0.17 h / 20 °C

4.2: 12 h / 20 °C

5.1: hydrogenchloride / water; tetrahydrofuran / 12 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; formic acid; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja4025148

Reference yield:

: 1438020-76-8
C₂₅H₃₄N₂O₅

: 1438021-20-5
C₂₂H₂₉N₅O₄*ClH

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid; hydrogenchloride / dichloromethane; water / 12 h / 20 °C

2.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; 4-methyl-morpholine / N,N-dimethyl-formamide / 0.17 h / 20 °C

2.2: 12 h / 20 °C

3.1: hydrogenchloride / water; tetrahydrofuran / 12 h / 20 °C

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja4025148