rac-N-3-(3-pyridine)propionyl-p-toluene-sulfinamide

Base Information

Chemical Name:rac-N-3-(3-pyridine)propionyl-p-toluene-sulfinamide
CAS No.:934631-21-7
Molecular Formula:C₁₅H₁₆N₂O₂S
Molecular Weight:288.37
Hs Code.:

Synonyms:rac-N-3-(3-pyridine)propionyl-p-toluene-sulfinamide

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Chemical Property of rac-N-3-(3-pyridine)propionyl-p-toluene-sulfinamide

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Technology Process of rac-N-3-(3-pyridine)propionyl-p-toluene-sulfinamide

There total 3 articles about rac-N-3-(3-pyridine)propionyl-p-toluene-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 3724-19-4
3-pyridine propionic acid

: 6873-55-8
p-tolylsulfinyl amide

: 934631-21-7
rac-N-3-(3-pyridine)propionyl-p-toluene-sulfinamide

Guidance literature:: p-tolylsulfinyl amide; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.25h;

3-pyridine propionic acid; In tetrahydrofuran; at 20 ℃; for 3h;
DOI:10.1002/adsc.200606040

Reference yield:

: 2859-67-8
3-(3-pyridyl)propan-1-ol

: 934631-21-7
rac-N-3-(3-pyridine)propionyl-p-toluene-sulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 70 percent / KMnO₄; aq. H₂SO₄ / 24 h / 20 °C

2.1: NaH / tetrahydrofuran / 0.25 h / 0 °C

2.2: 73 percent / tetrahydrofuran / 3 h / 20 °C

With potassium permanganate; sulfuric acid; sodium hydride; In tetrahydrofuran;
DOI:10.1002/adsc.200606040

Reference yield:

: 824-79-3
sodium 4-methylbenzenesulfinate

: 934631-21-7
rac-N-3-(3-pyridine)propionyl-p-toluene-sulfinamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: oxalyl chloride / toluene / 1 h / 20 °C

1.2: 86 percent / NH₄OH / toluene; ethyl acetate / 1 h / 20 °C

2.1: NaH / tetrahydrofuran / 0.25 h / 0 °C

2.2: 73 percent / tetrahydrofuran / 3 h / 20 °C

With oxalyl dichloride; sodium hydride; In tetrahydrofuran; toluene;
DOI:10.1002/adsc.200606040