methyl [2-O-benzoyl-3-O-benzyl-4-O-(1-naphthylmethyl)-β-D-glucopyranosyl]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

Base Information

• Chemical Name: methyl [2-O-benzoyl-3-O-benzyl-4-O-(1-naphthylmethyl)-β-D-glucopyranosyl]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)
• CAS No.: 1253183-69-5
• Molecular Formula: C₅₄H₅₇NO₁₂
• Molecular Weight: 912.046

Synonyms:methyl [2-O-benzoyl-3-O-benzyl-4-O-(1-naphthylmethyl)-β-D-glucopyranosyl]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

Chemical Property of methyl [2-O-benzoyl-3-O-benzyl-4-O-(1-naphthylmethyl)-β-D-glucopyranosyl]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

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Technology Process of methyl [2-O-benzoyl-3-O-benzyl-4-O-(1-naphthylmethyl)-β-D-glucopyranosyl]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

There total 1 articles about methyl [2-O-benzoyl-3-O-benzyl-4-O-(1-naphthylmethyl)-β-D-glucopyranosyl]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

methyl [2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-4-O-(1-naphthylmethyl)-β-D-glucopyranosyl]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside) (1253183-68-4) → methyl [2-O-benzoyl-3-O-benzyl-4-O-(1-naphthylmethyl)-β-D-glucopyranosyl]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside) (1253183-69-5)

Guidance literature:

With dithiocarbonic acid hydrazide; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

DOI:10.1016/j.tet.2010.08.004

Reference yield: 73.0%

methyl [2-O-benzoyl-3-O-benzyl-4-O-(1-naphthylmethyl)-β-D-glucopyranosyl]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside) (1253183-69-5) + tert-butyl alcohol (75-65-0) → methyl {tert-butyl [2-O-benzoyl-3-O-benzyl-4-O-(1-naphthylmethyl)-β-D-glucopyranosyl]uronate}-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside) (1253183-71-9)

Guidance literature:

With dipyridinium dichromate; acetic anhydride; In dichloromethane; at 20 ℃; for 6h;

DOI:10.1016/j.tet.2010.08.004

upstream raw materials:

methyl [2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-4-O-(1-naphthylmethyl)-β-D-glucopyranosyl]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

Downstream raw materials:

methyl {tert-butyl [2-O-benzoyl-3-O-benzyl-4-O-(1-naphthylmethyl)-β-D-glucopyranosyl]uronate}-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

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