Diphenyl (N-methylthiocarbamoyl)thionophosphonate

Base Information

Chemical Name:Diphenyl (N-methylthiocarbamoyl)thionophosphonate
CAS No.:86835-83-8
Molecular Formula:C₁₄H₁₄NO₂PS₂
Molecular Weight:323.376
Hs Code.:

Synonyms:Diphenyl (N-methylthiocarbamoyl)thionophosphonate

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Chemical Property of Diphenyl (N-methylthiocarbamoyl)thionophosphonate

Chemical Property:

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Technology Process of Diphenyl (N-methylthiocarbamoyl)thionophosphonate

There total 3 articles about Diphenyl (N-methylthiocarbamoyl)thionophosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 58045-33-3
diphenyl thiophosphonate

: 556-61-6
methyl thioisocyanate

: 86835-83-8
Diphenyl (N-methylthiocarbamoyl)thionophosphonate

Guidance literature:: With triethylamine; at 75 ℃; for 0.333333h;
DOI:10.1021/jo00170a018

Reference yield: 30.0%

: 81940-07-0
diphenyl (N-methylthiocarbamoyl)phosphonate

: 86835-83-8
Diphenyl (N-methylthiocarbamoyl)thionophosphonate

Guidance literature:: With tetraphosphorus decasulfide; In toluene; for 1.5h; Heating;
DOI:10.1021/jo00170a018

Reference yield:

: 4712-55-4
diphenyl hydrogen phosphite

: 86835-83-8
Diphenyl (N-methylthiocarbamoyl)thionophosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / P₄S₁₀ / 2 h / 90 °C

2: 70 percent / Et₃N / 0.33 h / 75 °C

With tetraphosphorus decasulfide; triethylamine;
DOI:10.1021/jo00170a018