2-(R)-(7-methoxy-2,3-dihydro-isoindol-1-one-2-ylmethyl)-4-oxo-1-(1-(S)-phenyl-ethyl)-piperidine

Base Information

• Chemical Name: 2-(R)-(7-methoxy-2,3-dihydro-isoindol-1-one-2-ylmethyl)-4-oxo-1-(1-(S)-phenyl-ethyl)-piperidine
• CAS No.: 330194-40-6
• Molecular Formula: C₂₃H₂₆N₂O₃
• Molecular Weight: 378.471

Synonyms:2-(R)-(7-methoxy-2,3-dihydro-isoindol-1-one-2-ylmethyl)-4-oxo-1-(1-(S)-phenyl-ethyl)-piperidine

Chemical Property of 2-(R)-(7-methoxy-2,3-dihydro-isoindol-1-one-2-ylmethyl)-4-oxo-1-(1-(S)-phenyl-ethyl)-piperidine

Chemical Property:

Purity/Quality:

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Technology Process of 2-(R)-(7-methoxy-2,3-dihydro-isoindol-1-one-2-ylmethyl)-4-oxo-1-(1-(S)-phenyl-ethyl)-piperidine

There total 2 articles about 2-(R)-(7-methoxy-2,3-dihydro-isoindol-1-one-2-ylmethyl)-4-oxo-1-(1-(S)-phenyl-ethyl)-piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-(R)-(7-methoxy-2,3-dihydro-isoindol-1-one-2-ylmethyl)-4,4-diethoxy-1-(1-(S)-phenyl-ethyl)-piperidine (330194-39-3) → 2-(R)-(7-methoxy-2,3-dihydro-isoindol-1-one-2-ylmethyl)-4-oxo-1-(1-(S)-phenyl-ethyl)-piperidine (330194-40-6)

Guidance literature:

With trifluoroacetic acid; In water; at 0 ℃; for 0.5h;

Reference yield:

2-(R)-(7-methoxy-2,3-dihydro-isoindol-1-one-2-ylmethyl)-4,4-diethoxy-1-(1-(S)-phenyl-ethyl)-piperidine (330194-39-3) + sodium carbonate (497-19-8) → 2-(R)-(7-methoxy-2,3-dihydro-isoindol-1-one-2-ylmethyl)-4-oxo-1-(1-(S)-phenyl-ethyl)-piperidine (330194-40-6)

Guidance literature:

With trifluoroacetic acid; In water;

Reference yield:

2-(R)-(7-methoxy-2,3-dihydro-isoindol-1-one-2-ylmethyl)-4-oxo-1-(1-(S)-phenyl-ethyl)-piperidine (330194-40-6) + cyanoacetic acid tert-butyl ester (1116-98-9) → 2-amino-5-(R)-(7-methoxy-1-oxo-1,3-dihydro-isoindol-2-ylmethyl)-6-(1-(S)-phenyl-ethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylic acid tert-butyl ester (330194-41-7) + 2-amino-7-(S)-(7-methoxy-1-oxo-1,3-dihydro-isoindol-2-ylmethyl)-6-(1-(S)-phenyl-ethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylic acid tert-butyl ester (330194-42-8)

Guidance literature:

With 4-methyl-morpholine; sulfur; In ethanol; at 50 ℃; for 16h; Molecular sieve;

upstream raw materials:

2-(R)-(7-methoxy-2,3-dihydro-isoindol-1-one-2-ylmethyl)-4,4-diethoxy-1-(1-(S)-phenyl-ethyl)-piperidine

sodium carbonate

Downstream raw materials:

2-amino-5-(R)-(7-methoxy-1-oxo-1,3-dihydro-isoindol-2-ylmethyl)-6-(1-(S)-phenyl-ethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylic acid tert-butyl ester

2-amino-7-(S)-(7-methoxy-1-oxo-1,3-dihydro-isoindol-2-ylmethyl)-6-(1-(S)-phenyl-ethyl)-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylic acid tert-butyl ester

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