4,4',4'',4'''-(pyrene-1,3,6,8-tetrayl)tetrabenzaldehyde

Base Information

Chemical Name:4,4',4'',4'''-(pyrene-1,3,6,8-tetrayl)tetrabenzaldehyde
CAS No.:1415238-25-3
Molecular Formula:C₄₄H₂₆O₄
Molecular Weight:618.688
Hs Code.:
Mol file:1415238-25-3.mol

Synonyms:4,4',4'',4'''-(pyrene-1,3,6,8-tetrayl)tetrabenzaldehyde

Suppliers and Price of 4,4',4'',4'''-(pyrene-1,3,6,8-tetrayl)tetrabenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Ambeed
4,4',4'',4'''-(Pyrene-1,3,6,8-tetrayl)tetrabenzaldehyde 99%
5g
$ 550.00

Ambeed
4,4',4'',4'''-(Pyrene-1,3,6,8-tetrayl)tetrabenzaldehyde 99%
1g
$ 138.00

Ambeed
4,4',4'',4'''-(Pyrene-1,3,6,8-tetrayl)tetrabenzaldehyde 99%
250mg
$ 48.00

Ambeed
4,4',4'',4'''-(Pyrene-1,3,6,8-tetrayl)tetrabenzaldehyde 99%
100mg
$ 28.00

Total 20 raw suppliers

Chemical Property of 4,4',4'',4'''-(pyrene-1,3,6,8-tetrayl)tetrabenzaldehyde

Chemical Property:

Boiling Point:811.7±65.0 °C(Predicted)
Density:1.316±0.06 g/cm3(Predicted)
Storage Temp.:under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

4,4',4'',4'''-(Pyrene-1,3,6,8-tetrayl)tetrabenzaldehyde 99% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses 4,4',4'',4'''-(pyrene-1,3,6,8-tetrayl)tetrabenzaldehyde is a polycyclic aromatic hydrocarbon compound and can be used as a pharmaceutical intermediate.

Technology Process of 4,4',4'',4'''-(pyrene-1,3,6,8-tetrayl)tetrabenzaldehyde

There total 3 articles about 4,4',4'',4'''-(pyrene-1,3,6,8-tetrayl)tetrabenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: C₆₄H₆₆O₈

: 1415238-25-3
4,4',4'',4'''-(pyrene-1,3,6,8-tetrayl)tetrabenzaldehyde

Guidance literature:: With trifluoroacetic acid; In chloroform; water; at 20 ℃; for 16h;
DOI:10.1021/jacs.9b08079

Reference yield: 81.0%

: 128-63-2
1,3,6,8-tetrabromopyrene

: 87199-17-5
4-formylphenylboronic acid,

: 1415238-25-3
4,4',4'',4'''-(pyrene-1,3,6,8-tetrayl)tetrabenzaldehyde

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate; In tetrahydrofuran; water; for 24h; Inert atmosphere; Reflux;
DOI:10.1021/acs.joc.1c01260

Reference yield:

: 129-00-0
pyrene

: 1415238-25-3
4,4',4'',4'''-(pyrene-1,3,6,8-tetrayl)tetrabenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / nitrobenzene / 110 °C

2: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / 110 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromine; potassium carbonate; In 1,4-dioxane; nitrobenzene; 2: |Suzuki Coupling;
DOI:10.1039/c9cc08107k