2-azidoethyl 4:6-O-phenylmethylene-β-D-galactopyranosyl-(1→4)-β-D-glucopyranoside

Base Information

Chemical Name:2-azidoethyl 4:6-O-phenylmethylene-β-D-galactopyranosyl-(1→4)-β-D-glucopyranoside
CAS No.:702686-16-6
Molecular Formula:C₂₁H₂₉N₃O₁₁
Molecular Weight:499.475
Hs Code.:

Synonyms:2-azidoethyl 4:6-O-phenylmethylene-β-D-galactopyranosyl-(1→4)-β-D-glucopyranoside

Suppliers and Price of 2-azidoethyl 4:6-O-phenylmethylene-β-D-galactopyranosyl-(1→4)-β-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-azidoethyl 4:6-O-phenylmethylene-β-D-galactopyranosyl-(1→4)-β-D-glucopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of 2-azidoethyl 4:6-O-phenylmethylene-β-D-galactopyranosyl-(1→4)-β-D-glucopyranoside

There total 6 articles about 2-azidoethyl 4:6-O-phenylmethylene-β-D-galactopyranosyl-(1→4)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.2%

: 1125-88-8
benzaldehyde dimethyl acetal

: 230286-11-0
2-azidoethyl β-D-galactopyranosyl-(1->4)-β-D-glucopyranoside

: 702686-16-6
2-azidoethyl 4:6-O-phenylmethylene-β-D-galactopyranosyl-(1→4)-β-D-glucopyranoside

Guidance literature:: With camphor-10-sulfonic acid; In acetonitrile; at 0 - 20 ℃;
DOI:10.1039/c5ra00759c

Reference yield:

: 937400-94-7
2-azidoethyl β-D-glucopyranosyl-(1,4)-β-D-glucopyranoside

: 1125-88-8
benzaldehyde dimethyl acetal

: 702686-16-6
2-azidoethyl 4:6-O-phenylmethylene-β-D-galactopyranosyl-(1→4)-β-D-glucopyranoside

Guidance literature:: With camphor-10-sulfonic acid; In toluene; at 80 ℃; for 3h; regioselective reaction; Inert atmosphere;
DOI:10.1007/s11426-013-4838-4

Reference yield:

: 873199-49-6
Acetic acid (2R,3R,4S,5R,6R)-3-acetoxy-6-acetoxymethyl-2-(2-azido-ethoxy)-5-((2S,3R,4S,5R,6R)-3,4,5-triacetoxy-6-acetoxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-4-yl ester

: 702686-16-6
2-azidoethyl 4:6-O-phenylmethylene-β-D-galactopyranosyl-(1→4)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate / methanol / 5 h / Inert atmosphere

2: camphor-10-sulfonic acid / toluene / 3 h / 80 °C / Inert atmosphere

With camphor-10-sulfonic acid; sodium methylate; In methanol; toluene;
DOI:10.1007/s11426-013-4838-4