N-carbobenzyloxy-L-phenylalanine isopentylamide

Base Information

Chemical Name:N-carbobenzyloxy-L-phenylalanine isopentylamide
CAS No.:110755-28-7
Molecular Formula:C₂₂H₂₈N₂O₃
Molecular Weight:368.476
Hs Code.:

Synonyms:N-carbobenzyloxy-L-phenylalanine isopentylamide

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Chemical Property of N-carbobenzyloxy-L-phenylalanine isopentylamide

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Technology Process of N-carbobenzyloxy-L-phenylalanine isopentylamide

There total 1 articles about N-carbobenzyloxy-L-phenylalanine isopentylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 110755-28-7
N-carbobenzyloxy-L-phenylalanine isopentylamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylmorpholine / CH₂Cl₂ / 0.5 h / -15 °C

2: CH₂Cl₂ / 15 h / 4 °C

With 4-methyl-morpholine; In dichloromethane;
DOI:10.1016/0223-5234(92)90018-V

Reference yield: 90.0%

: 110755-28-7
N-carbobenzyloxy-L-phenylalanine isopentylamide

: 110755-29-8
L-phenylalanylamido(3-methyl)butane

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 4h;
DOI:10.1016/0223-5234(92)90018-V

Reference yield:

: 110755-28-7
N-carbobenzyloxy-L-phenylalanine isopentylamide

: N-iodoacetyl-L-phenylalanine isopentylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / H₂ / 10percent Pd/C / methanol / 4 h

2: 91 percent / dicyclohexylcarbodiimide, 1-hydroxybenzotriazole / CH₂Cl₂

With hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/0223-5234(92)90018-V