Technology Process of C19H18F2N8O2S
There total 7 articles about C19H18F2N8O2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
1-methyl-pyrrolidin-2-one;
at 50 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: potassium nitrate; sulfuric acid / water / -10 - 20 °C
2: hydrogen / palladium 10% on activated carbon / methanol / 3 h / 10343.2 Torr / Autoclave
3: pyridine / dichloromethane / 16 h / 20 °C
4: hydrogenchloride / ethanol; water / 2 h / 80 °C
5: acetic acid / methanol / 2 h / 50 °C
6: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 20 °C
7: N-ethyl-N,N-diisopropylamine / 1-methyl-pyrrolidin-2-one / 16 h / 50 °C
With
pyridine; hydrogenchloride; sulfuric acid; hydrogen; acetic acid; potassium nitrate; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
palladium 10% on activated carbon;
In
1-methyl-pyrrolidin-2-one; methanol; ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: hydrogen / palladium 10% on activated carbon / methanol / 3 h / 10343.2 Torr / Autoclave
2: pyridine / dichloromethane / 16 h / 20 °C
3: hydrogenchloride / ethanol; water / 2 h / 80 °C
4: acetic acid / methanol / 2 h / 50 °C
5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 20 °C
6: N-ethyl-N,N-diisopropylamine / 1-methyl-pyrrolidin-2-one / 16 h / 50 °C
With
pyridine; hydrogenchloride; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid;
palladium 10% on activated carbon;
In
1-methyl-pyrrolidin-2-one; methanol; ethanol; dichloromethane; water;