trans-{4-[6-butyl-5-(4-cyclohexyloxyphenyl)pyridazin-3-yloxy]cyclohexyl}carbamic acid tert-butyl ester

Base Information

Chemical Name:trans-{4-[6-butyl-5-(4-cyclohexyloxyphenyl)pyridazin-3-yloxy]cyclohexyl}carbamic acid tert-butyl ester
CAS No.:1331775-90-6
Molecular Formula:C₃₁H₄₅N₃O₄
Molecular Weight:523.716
Hs Code.:

Synonyms:trans-{4-[6-butyl-5-(4-cyclohexyloxyphenyl)pyridazin-3-yloxy]cyclohexyl}carbamic acid tert-butyl ester

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Chemical Property of trans-{4-[6-butyl-5-(4-cyclohexyloxyphenyl)pyridazin-3-yloxy]cyclohexyl}carbamic acid tert-butyl ester

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Technology Process of trans-{4-[6-butyl-5-(4-cyclohexyloxyphenyl)pyridazin-3-yloxy]cyclohexyl}carbamic acid tert-butyl ester

There total 2 articles about trans-{4-[6-butyl-5-(4-cyclohexyloxyphenyl)pyridazin-3-yloxy]cyclohexyl}carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-32-1
octanoic acid ethyl ester

: 1331775-90-6
trans-{4-[6-butyl-5-(4-cyclohexyloxyphenyl)pyridazin-3-yloxy]cyclohexyl}carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrazine hydrate; acetic acid / 12 h / 100 °C

2.1: trichlorophosphate; 2H-Pyridazin-3-one / 0.5 h / 90 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C

3.2: 3 h / 50 °C

With 2H-Pyridazin-3-one; sodium hydride; hydrazine hydrate; acetic acid; trichlorophosphate; In tetrahydrofuran; mineral oil;

Reference yield:

: 1331775-51-9
6-butyl-5-(4-cyclohexyloxyphenyl)-2H-pyridazin-3-one

: 1331775-90-6
trans-{4-[6-butyl-5-(4-cyclohexyloxyphenyl)pyridazin-3-yloxy]cyclohexyl}carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorophosphate; 2H-Pyridazin-3-one / 0.5 h / 90 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C

2.2: 3 h / 50 °C

With 2H-Pyridazin-3-one; sodium hydride; trichlorophosphate; In tetrahydrofuran; mineral oil;