N1-(5-monomethoxytrityloxyethoxyethyl)-5'-O-(tert-butyl-dimethylsilyl)-2',3'-O-isopropylideneinosine

Base Information

Chemical Name:N1-(5-monomethoxytrityloxyethoxyethyl)-5'-O-(tert-butyl-dimethylsilyl)-2',3'-O-isopropylideneinosine
CAS No.:1232139-67-1
Molecular Formula:C₄₃H₅₄N₄O₈Si
Molecular Weight:783.009
Hs Code.:

Synonyms:N1-(5-monomethoxytrityloxyethoxyethyl)-5'-O-(tert-butyl-dimethylsilyl)-2',3'-O-isopropylideneinosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N1-(5-monomethoxytrityloxyethoxyethyl)-5'-O-(tert-butyl-dimethylsilyl)-2',3'-O-isopropylideneinosine

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Technology Process of N1-(5-monomethoxytrityloxyethoxyethyl)-5'-O-(tert-butyl-dimethylsilyl)-2',3'-O-isopropylideneinosine

There total 3 articles about N1-(5-monomethoxytrityloxyethoxyethyl)-5'-O-(tert-butyl-dimethylsilyl)-2',3'-O-isopropylideneinosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1232139-65-9
N1-[(5-hydroxyl)ethoxyethyl]-5'-O-(tert-butyldimethylsilyl)-2',3'-O-isopropylideneinosine

: 14470-28-1
mono-4-methoxytrityl chloride

: 1232139-67-1
N1-(5-monomethoxytrityloxyethoxyethyl)-5'-O-(tert-butyl-dimethylsilyl)-2',3'-O-isopropylideneinosine

Guidance literature:: With pyridine; at 20 ℃; for 8h;
DOI:10.1039/b9nj00595a

Reference yield:

: 1072463-01-4
C₂₅H₃₂N₆O₉Si

: 1232139-67-1
N1-(5-monomethoxytrityloxyethoxyethyl)-5'-O-(tert-butyl-dimethylsilyl)-2',3'-O-isopropylideneinosine

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 8 h / 50 °C

2: pyridine / 8 h / 20 °C

With pyridine; In N,N-dimethyl-formamide;
DOI:10.1039/b9nj00595a

Reference yield:

: 5'-O-TBDMS-2',3'-O-isopropylideneinosine

: 1232139-67-1
N1-(5-monomethoxytrityloxyethoxyethyl)-5'-O-(tert-butyl-dimethylsilyl)-2',3'-O-isopropylideneinosine

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 80 °C

2: N,N-dimethyl-formamide / 8 h / 50 °C

3: pyridine / 8 h / 20 °C

With pyridine; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1039/b9nj00595a