1-[(ethoxycarbonothioyl)thio]-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl pivalate

Base Information

Chemical Name:1-[(ethoxycarbonothioyl)thio]-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl pivalate
CAS No.:1509927-90-5
Molecular Formula:C₂₂H₃₁NO₆S₃
Molecular Weight:501.689
Hs Code.:

Synonyms:1-[(ethoxycarbonothioyl)thio]-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl pivalate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[(ethoxycarbonothioyl)thio]-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl pivalate

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Technology Process of 1-[(ethoxycarbonothioyl)thio]-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl pivalate

There total 4 articles about 1-[(ethoxycarbonothioyl)thio]-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 3377-92-2,26715-88-8
vinyl pivalate

: 1101206-99-8
dithiocarbonic acid O-ethyl ester S-[4-oxo-1-(toluene-4-sulfonyl)-piperidin-3-yl]ester

: 1509927-90-5
1-[(ethoxycarbonothioyl)thio]-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl pivalate

Guidance literature:: With dilauryl peroxide; In ethyl acetate; Inert atmosphere; Reflux;
DOI:10.1021/ol403310f

Reference yield:

: 171009-41-9
O-ethyl-S-(4-oxo-1-tosylpiperidin-3-yl)carbonodithioate

: 1509927-90-5
1-[(ethoxycarbonothioyl)thio]-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl pivalate

Guidance literature:: Multi-step reaction with 2 steps

1: acetone / 0 - 20 °C / Inert atmosphere

2: dilauryl peroxide / ethyl acetate / Inert atmosphere; Reflux

With dilauryl peroxide; In ethyl acetate; acetone;
DOI:10.1021/ol403310f

Reference yield:

: 1332708-91-4
C₁₅H₂₃NO₃SSi

: 1509927-90-5
1-[(ethoxycarbonothioyl)thio]-2-(4-oxo-1-tosylpiperidin-3-yl)ethyl pivalate

Guidance literature:: Multi-step reaction with 3 steps

1: N-Bromosuccinimide / tetrahydrofuran / 0.08 h / 0 °C

2: acetone / 0 - 20 °C / Inert atmosphere

3: dilauryl peroxide / ethyl acetate / Inert atmosphere; Reflux

With N-Bromosuccinimide; dilauryl peroxide; In tetrahydrofuran; ethyl acetate; acetone;
DOI:10.1021/ol403310f