2(1H)-Pyridinethione, 3,6-dihydro-1-methyl-6-(2-propen-1-yl)-

Base Information

Chemical Name:2(1H)-Pyridinethione, 3,6-dihydro-1-methyl-6-(2-propen-1-yl)-
CAS No.:859845-73-1
Molecular Formula:C₉H₁₃NS
Molecular Weight:167.275
Hs Code.:
Mol file:859845-73-1.mol

Synonyms:2(1H)-Pyridinethione,3,6-dihydro-1-methyl-6-(2-propenyl)- (9CI)

Suppliers and Price of 2(1H)-Pyridinethione, 3,6-dihydro-1-methyl-6-(2-propen-1-yl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2(1H)-Pyridinethione, 3,6-dihydro-1-methyl-6-(2-propen-1-yl)-

Chemical Property:

PSA：35.33000
LogP:2.08810

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2(1H)-Pyridinethione, 3,6-dihydro-1-methyl-6-(2-propen-1-yl)-

There total 3 articles about 2(1H)-Pyridinethione, 3,6-dihydro-1-methyl-6-(2-propen-1-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 2044-27-1
1-methyl-2-pyridinethione

: 2622-05-1
allylmagnesium bromide

: 859845-73-1
6-allyl-1-methyl-3,6-dihydro-1H-pyridine-2-thione

Guidance literature:: allylmagnesium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at 0 ℃; for 0.166667h;

1-methyl-2-pyridinethione; In tetrahydrofuran; hexane; at -72 ℃; for 0.5h; Further stages.;
DOI:10.1016/j.tet.2007.09.029

Reference yield:

: 2044-27-1
1-methyl-2-pyridinethione

: 2622-05-1
allylmagnesium bromide

4-allyl-1-methyl-3,4-dihydro-1H-pyridine-2-thione: 4-allyl-1-methyl-3,4-dihydro-1H-pyridine-2-thione

: 859845-73-1
6-allyl-1-methyl-3,6-dihydro-1H-pyridine-2-thione

Guidance literature:: With n-butyllithium; In tetrahydrofuran; pentane; at 0 ℃; for 0.5h;
DOI:10.1016/j.tetlet.2005.04.097

Reference yield:

: 2044-27-1
1-methyl-2-pyridinethione

: 24850-33-7
allyltributylstanane

4-allyl-1-methyl-3,4-dihydro-1H-pyridine-2-thione: 4-allyl-1-methyl-3,4-dihydro-1H-pyridine-2-thione

: 859845-73-1
6-allyl-1-methyl-3,6-dihydro-1H-pyridine-2-thione

Guidance literature:: allyltributylstanane; With n-butyllithium; In hexane; at 20 ℃; for 0.5h;

1-methyl-2-pyridinethione; In tetrahydrofuran; hexane; at -70 ℃; for 0.5h; Further stages.;
DOI:10.1016/j.tet.2007.09.029