Acetoxy-benzoylamino-acetic acid (E)-3-phenyl-allyl ester

Base Information

Chemical Name:Acetoxy-benzoylamino-acetic acid (E)-3-phenyl-allyl ester
CAS No.:112654-48-5
Molecular Formula:C₂₀H₁₉NO₅
Molecular Weight:353.375
Hs Code.:

Synonyms:Acetoxy-benzoylamino-acetic acid (E)-3-phenyl-allyl ester

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Chemical Property of Acetoxy-benzoylamino-acetic acid (E)-3-phenyl-allyl ester

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Technology Process of Acetoxy-benzoylamino-acetic acid (E)-3-phenyl-allyl ester

There total 6 articles about Acetoxy-benzoylamino-acetic acid (E)-3-phenyl-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 108-24-7
acetic anhydride

: 112654-64-5
Benzoylamino-hydroxy-acetic acid (E)-3-phenyl-allyl ester

: 112654-48-5
Acetoxy-benzoylamino-acetic acid (E)-3-phenyl-allyl ester

Guidance literature:: With pyridine; dmap; In dichloromethane; for 0.0833333h;
DOI:10.1021/jo00239a031

Reference yield:

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 112654-48-5
Acetoxy-benzoylamino-acetic acid (E)-3-phenyl-allyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 73 percent / pyridine / CH₂Cl₂ / 0.33 h / 0 °C

2: 94 percent / silver nitrate / acetonitrile / 24 h

3: 92 percent / sodium acetate / dimethylsulfoxide / 0.42 h

4: 60 percent / acetone / 72 h / Ambient temperature

5: 90 percent / pyridine, 4-(dimethylamino)pyridine / CH₂Cl₂ / 0.08 h

With pyridine; dmap; sodium acetate; silver nitrate; In dichloromethane; dimethyl sulfoxide; acetone; acetonitrile;
DOI:10.1021/jo00239a031

Reference yield:

: 55-21-0,27208-38-4
benzamide

: 112654-48-5
Acetoxy-benzoylamino-acetic acid (E)-3-phenyl-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / acetone / 72 h / Ambient temperature

2: 90 percent / pyridine, 4-(dimethylamino)pyridine / CH₂Cl₂ / 0.08 h

With pyridine; dmap; In dichloromethane; acetone;
DOI:10.1021/jo00239a031