(2S,3S)-3,4-O-isopropylidene-2-O-methanesulfonyl-1-O-p-methoxybenzylthreitol

Base Information

Chemical Name:(2S,3S)-3,4-O-isopropylidene-2-O-methanesulfonyl-1-O-p-methoxybenzylthreitol
CAS No.:177957-86-7
Molecular Formula:C₁₆H₂₄O₇S
Molecular Weight:360.428
Hs Code.:

Synonyms:(2S,3S)-3,4-O-isopropylidene-2-O-methanesulfonyl-1-O-p-methoxybenzylthreitol

Suppliers and Price of (2S,3S)-3,4-O-isopropylidene-2-O-methanesulfonyl-1-O-p-methoxybenzylthreitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-3,4-O-isopropylidene-2-O-methanesulfonyl-1-O-p-methoxybenzylthreitol

Chemical Property:

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Technology Process of (2S,3S)-3,4-O-isopropylidene-2-O-methanesulfonyl-1-O-p-methoxybenzylthreitol

There total 4 articles about (2S,3S)-3,4-O-isopropylidene-2-O-methanesulfonyl-1-O-p-methoxybenzylthreitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 124-63-0
methanesulfonyl chloride

: 177957-85-6
(2S,3S)-3,4-O-isopropylidene-1-O-p-methoxybenzylthreitol

: 177957-86-7
(2S,3S)-3,4-O-isopropylidene-2-O-methanesulfonyl-1-O-p-methoxybenzylthreitol

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃;
DOI:10.1016/0040-4039(96)00594-1

Reference yield:

: 84379-53-3
2-O-benzyl-3,4-O-isopropylidene-L-threitol

: 177957-86-7
(2S,3S)-3,4-O-isopropylidene-2-O-methanesulfonyl-1-O-p-methoxybenzylthreitol

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / NaH / paraffin; dimethylformamide; tetrahydrofuran / 1.5 h / Ambient temperature

2: 93 percent / H₂ / Raney Ni / ethanol / 1 h / 760 Torr / Ambient temperature

3: 100 percent / Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

With hydrogen; sodium hydride; triethylamine; nickel; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; paraffin;
DOI:10.1016/S0040-4020(97)00651-0

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 177957-86-7
(2S,3S)-3,4-O-isopropylidene-2-O-methanesulfonyl-1-O-p-methoxybenzylthreitol

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / NaH / paraffin; dimethylformamide; tetrahydrofuran / 1.5 h / Ambient temperature

2: 93 percent / H₂ / Raney Ni / ethanol / 1 h / 760 Torr / Ambient temperature

3: 100 percent / Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

With hydrogen; sodium hydride; triethylamine; nickel; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; paraffin;
DOI:10.1016/S0040-4020(97)00651-0