(S)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid, dicyclohexylamine salt

Base Information

Chemical Name:(S)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid, dicyclohexylamine salt
CAS No.:1265819-93-9
Molecular Formula:C₁₂H₂₃N*C₁₅H₁₉ClO₄S
Molecular Weight:512.154
Hs Code.:

Synonyms:(S)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid, dicyclohexylamine salt

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Chemical Property of (S)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid, dicyclohexylamine salt

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Technology Process of (S)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid, dicyclohexylamine salt

There total 2 articles about (S)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid, dicyclohexylamine salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (E)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-acrylic acid, dicyclohexylamine salt

: 1265819-90-6
(R)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid, dicyclohexylamine salt

: 1265819-93-9
(S)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid, dicyclohexylamine salt

Guidance literature:: With hydrogen; Ru(OAc)2((R)-DiMeOBIPHEP); In methanol; at 50 ℃; under 37503.8 Torr; Product distribution / selectivity; Autoclave;

Reference yield:

: 87776-75-8
(3-chloro-4-methylsulfanyl-phenyl)-acetic acid

: 1265819-90-6
(R)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid, dicyclohexylamine salt

: 1265819-93-9
(S)-2-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionic acid, dicyclohexylamine salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: formic acid; dihydrogen peroxide / water / 16 h / 50 °C

2.1: acetic anhydride; sodium acetate / tetrahydrofuran / 24 h / 40 °C

2.2: 2 h / 40 °C

2.3: pH 6

3.1: acetone / 17 h / 20 °C

4.1: hydrogen / Ru(TFA)2((S)-TriMeOBIPHEP) / methanol / 50 °C / 37503.8 Torr / Autoclave

With formic acid; hydrogen; dihydrogen peroxide; sodium acetate; acetic anhydride; Ru(TFA)2((S)-TriMeOBIPHEP); In tetrahydrofuran; methanol; water; acetone;