8-Benzyl-1c,6c-dimethoxycarbonyl-3,4-benzo-8-azabicyclo<4.3.1>dec-3-en-2,5-dion

Base Information

• Chemical Name: 8-Benzyl-1c,6c-dimethoxycarbonyl-3,4-benzo-8-azabicyclo<4.3.1>dec-3-en-2,5-dion
• CAS No.: 6506-21-4
• Molecular Formula: C₂₄H₂₃NO₆
• Molecular Weight: 421.45

Synonyms:8-Benzyl-1c,6c-dimethoxycarbonyl-3,4-benzo-8-azabicyclo<4.3.1>dec-3-en-2,5-dion

Chemical Property of 8-Benzyl-1c,6c-dimethoxycarbonyl-3,4-benzo-8-azabicyclo<4.3.1>dec-3-en-2,5-dion

Chemical Property:

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Technology Process of 8-Benzyl-1c,6c-dimethoxycarbonyl-3,4-benzo-8-azabicyclo<4.3.1>dec-3-en-2,5-dion

There total 2 articles about 8-Benzyl-1c,6c-dimethoxycarbonyl-3,4-benzo-8-azabicyclo<4.3.1>dec-3-en-2,5-dion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + 5H-benzocycloheptene-6,8-dicarboxylic acid-6,7,8,9-tetrahydro-5,9-dioxo-6,8-dimethyl ester (6496-77-1) + benzylamine (100-46-9) → 8-Benzyl-1c,6c-dimethoxycarbonyl-3,4-benzo-8-azabicyclo<4.3.1>dec-3-en-2,5-dion (6506-21-4) + 12-Methyl-2,9-dioxo-12-aza-tricyclo[8.3.1.03,8]tetradeca-3(8),4,6-triene-1,10-dicarboxylic acid dimethyl ester (6496-78-2)

Guidance literature:

With hydrogenchloride; at 90 ℃; for 40h;

DOI:10.1080/00397919708004806

Reference yield:

→ 8-Benzyl-1c,6c-dimethoxycarbonyl-3,4-benzo-8-azabicyclo<4.3.1>dec-3-en-2,5-dion (6506-21-4)

Guidance literature:

4,6-Dimethoxycarbonyl-1,2-benzo-cyclohept-1-en-3,7-dion (I), Dioxan, wss. Benzylamin, wss. Formaldehyd;

Reference yield: 36.0%

8-Benzyl-1c,6c-dimethoxycarbonyl-3,4-benzo-8-azabicyclo<4.3.1>dec-3-en-2,5-dion (6506-21-4) → phthalic acid dimethyl ester (131-11-3,64441-70-9) + (3R,5S)-1-Benzyl-piperidine-3,5-dicarboxylic acid dimethyl ester (175694-35-6) + (3S,5S)-1-Benzyl-piperidine-3,5-dicarboxylic acid dimethyl ester

Guidance literature:

With sodium; In methanol; at 100 ℃; for 30h;

DOI:10.1080/00397919708004806

upstream raw materials:

formaldehyd

5H-benzocycloheptene-6,8-dicarboxylic acid-6,7,8,9-tetrahydro-5,9-dioxo-6,8-dimethyl ester

benzylamine

Downstream raw materials:

phthalic acid dimethyl ester

(3R,5S)-1-Benzyl-piperidine-3,5-dicarboxylic acid dimethyl ester

dimethyl 1-benzyl-piperidine-3,5-dicarboxylate

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