Technology Process of C49H79ClO12Si
There total 4 articles about C49H79ClO12Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrahydrofuran / 0.5 h / -78 - 20 °C / Inert atmosphere
2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / Inert atmosphere
2.2: 0.5 h
3.1: dimethyl sulfide borane / tetrahydrofuran / 4 h / Inert atmosphere
With
dimethyl sulfide borane; 9-bora-bicyclo[3.3.1]nonane;
In
tetrahydrofuran;
1.1: Wittig olefination;
DOI:10.1039/c2ob25101a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / Inert atmosphere
2.1: tetrahydrofuran / 0.5 h / -78 - 20 °C / Inert atmosphere
3.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / Inert atmosphere
3.2: 0.5 h
4.1: dimethyl sulfide borane / tetrahydrofuran / 4 h / Inert atmosphere
With
dimethyl sulfide borane; sodium hydrogencarbonate; Dess-Martin periodane; 9-bora-bicyclo[3.3.1]nonane;
In
tetrahydrofuran; dichloromethane;
1.1: Dess-Martin oxidation / 2.1: Wittig olefination;
DOI:10.1039/c2ob25101a
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / Inert atmosphere
1.2: 0.5 h
2.1: dimethyl sulfide borane / tetrahydrofuran / 4 h / Inert atmosphere
With
dimethyl sulfide borane; 9-bora-bicyclo[3.3.1]nonane;
In
tetrahydrofuran;
DOI:10.1039/c2ob25101a
