Technology Process of C45H35NP2
There total 3 articles about C45H35NP2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
3,6-dibromo-9-(4-vinylbenzyl)-9H-carbazole;
With
n-butyllithium;
In
diethyl ether; hexane;
at -78 ℃;
for 1h;
chloro-diphenylphosphine;
In
diethyl ether; hexane;
at -78 - 20 ℃;
DOI:10.1016/j.polymer.2010.12.016
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tetraethylammonium bromide; potassium hydroxide / water; dimethyl sulfoxide / 0.5 h / 20 °C
1.2: 20 °C / Darkness
2.1: n-butyllithium / diethyl ether; hexane / 1 h / -78 °C
2.2: -78 - 20 °C
With
n-butyllithium; tetraethylammonium bromide; potassium hydroxide;
In
diethyl ether; hexane; water; dimethyl sulfoxide;
DOI:10.1016/j.polymer.2010.12.016
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: bromine; sodium acetate; acetic acid / 0 °C
2.1: tetraethylammonium bromide; potassium hydroxide / water; dimethyl sulfoxide / 0.5 h / 20 °C
2.2: 20 °C / Darkness
3.1: n-butyllithium / diethyl ether; hexane / 1 h / -78 °C
3.2: -78 - 20 °C
With
n-butyllithium; tetraethylammonium bromide; bromine; sodium acetate; acetic acid; potassium hydroxide;
In
diethyl ether; hexane; water; dimethyl sulfoxide;
DOI:10.1016/j.polymer.2010.12.016
