(-)-(1R,2R,5R)-5-iodo-2-methylcyclohexanecarboxylic acid

Base Information

Chemical Name:(-)-(1R,2R,5R)-5-iodo-2-methylcyclohexanecarboxylic acid
CAS No.:606933-64-6
Molecular Formula:C₈H₁₃IO₂
Molecular Weight:268.095
Hs Code.:

Synonyms:(-)-(1R,2R,5R)-5-iodo-2-methylcyclohexanecarboxylic acid

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Chemical Property of (-)-(1R,2R,5R)-5-iodo-2-methylcyclohexanecarboxylic acid

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Technology Process of (-)-(1R,2R,5R)-5-iodo-2-methylcyclohexanecarboxylic acid

There total 2 articles about (-)-(1R,2R,5R)-5-iodo-2-methylcyclohexanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 287178-31-8
(+)-(1R,2R,5R)-2-methyl-6-oxabicyclo[3.2.1]octan-7-one

: 606933-64-6
(-)-(1R,2R,5R)-5-iodo-2-methylcyclohexanecarboxylic acid

Guidance literature:: (+)-(1R,2R,5R)-2-methyl-6-oxabicyclo[3.2.1]octan-7-one; With Methyltrichlorosilane; sodium iodide; In acetonitrile; for 2h; Heating;

With sodium carbonate; In tetrahydrofuran; for 0.833333h; Heating;
DOI:10.1016/S0040-4020(03)00853-6

Reference yield:

: C₈H₁₃IO₂

: 287178-31-8
(+)-(1R,2R,5R)-2-methyl-6-oxabicyclo[3.2.1]octan-7-one

: 606933-64-6
(-)-(1R,2R,5R)-5-iodo-2-methylcyclohexanecarboxylic acid

Guidance literature:: C₈H₁₃IO₂; With potassium carbonate; In tetrahydrofuran; for 1h; Reflux;

With potassium carbonate; In water; at 0 ℃; pH=8 - 9;

Reference yield: 72.0%

: 64-17-5
ethanol

: 606933-64-6
(-)-(1R,2R,5R)-5-iodo-2-methylcyclohexanecarboxylic acid

: ethyl (-)-(1R,2R,5R)-5-iodo-trans-2-methylcyclohexanecarboxylate

Guidance literature:: (-)-(1R,2R,5R)-5-iodo-2-methylcyclohexanecarboxylic acid; With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; at 0 - 20 ℃; for 2h;

ethanol; With pyridine; In dichloromethane; at -10 - 20 ℃; for 2h;