C₂₅H₂₈N₆O₄S

Base Information

Chemical Name:C₂₅H₂₈N₆O₄S
CAS No.:1346243-88-6
Molecular Formula:C₂₅H₂₈N₆O₄S
Molecular Weight:508.601
Hs Code.:

C<sub>25</sub>H<sub>28</sub>N<sub>6</sub>O<sub>4</sub>S

Synonyms:C₂₅H₂₈N₆O₄S

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Chemical Property of C₂₅H₂₈N₆O₄S

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Technology Process of C₂₅H₂₈N₆O₄S

There total 7 articles about C₂₅H₂₈N₆O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1346243-08-0
N-(cyclopropylmethyl)-N-(3,5-dimethoxyphenyl)-3-(1H-pyrazol-4-yl)quinoxaline-6-amine

: 13360-57-1
dimethylamino sulfonyl chloride

: 1346243-88-6
C₂₅H₂₈N₆O₄S

Guidance literature:: With triethylamine; dmap; In dichloromethane; at 5 - 20 ℃; Inert atmosphere;

Reference yield:

: 10272-07-8
3.5-dimethoxyaniline

: 1346243-88-6
C₂₅H₂₈N₆O₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 5 °C / Inert atmosphere

3.2: 1.83 h / 5 - 20 °C

4.1: potassium phosphate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos / 1,4-dioxane; water / 80 °C / Inert atmosphere

5.1: hydrogenchloride; water / 1,4-dioxane / 70 °C

5.2: Cooling with ice

6.1: triethylamine / dmap / dichloromethane / 5 - 20 °C / Inert atmosphere

With hydrogenchloride; potassium phosphate; water; sodium hydride; triethylamine; sodium t-butanolate; trichlorophosphate; dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; XPhos; In 1,4-dioxane; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 82031-32-1
7-bromo-1H-quinoxalin-2-one

: 1346243-88-6
C₂₅H₂₈N₆O₄S

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.33 h / 5 °C / Inert atmosphere

3.2: 1.83 h / 5 - 20 °C

4.1: potassium phosphate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; XPhos / 1,4-dioxane; water / 80 °C / Inert atmosphere

5.1: hydrogenchloride; water / 1,4-dioxane / 70 °C

5.2: Cooling with ice

6.1: triethylamine / dmap / dichloromethane / 5 - 20 °C / Inert atmosphere

With hydrogenchloride; potassium phosphate; water; sodium hydride; triethylamine; sodium t-butanolate; trichlorophosphate; dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; XPhos; In 1,4-dioxane; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;