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N,N-Dimethylsulfamoyl chloride CAS:13360-57-1
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Dimethylsulfamoyl chloride
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Dimethylsulfamoyl chloride
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TIANFU-CHEM CAS:13360-57-1 Dimethylsulfamoyl chloride
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13360-57-1 Usage

Chemical Properties

clear colorless to slightly yellow liquid

Uses

Dichlorofluanid is a degradation product of the pesticide Dichlorofluanid.
InChI:InChI=1/C2H6ClNO2S/c1-4(2)7(3,5)6/h1-2H3

13360-57-1SDS

SAFETY DATA SHEETS

According to Globally Harmonized System of Classification and Labelling of Chemicals (GHS) - Sixth revised edition

Version: 1.0

Creation Date: Aug 10, 2017

Revision Date: Aug 10, 2017

1.Identification

1.1 GHS Product identifier

Product name Dimethylsulfamoyl chloride

1.2 Other means of identification

Product number -
Other names DiMethylsulfaMoyl Chloride

1.3 Recommended use of the chemical and restrictions on use

Identified uses For industry use only.
Uses advised against no data available

1.4 Supplier's details

1.5 Emergency phone number

Emergency phone number -
Service hours Monday to Friday, 9am-5pm (Standard time zone: UTC/GMT +8 hours).

More Details:13360-57-1 SDS

13360-57-1Synthetic route

N,N-dimethylammonium chloride

N,N-dimethylammonium chloride

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

dimethylchloroamine
1585-74-6

dimethylchloroamine

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

Conditions
ConditionsYield
With sulfur dioxide In tetrachloromethane 1.) 0 deg C, 1.5 h, 2.) up to r.t., overnight;70%
dimethyl amine
124-40-3

dimethyl amine

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

Conditions
ConditionsYield
With sulfuryl dichloride
With sulfuryl dichloride; triethylamine In 1,4-dioxane; chloroform at 0 - 20℃;
N,N-Dimethylcarbamoyl chloride
79-44-7

N,N-Dimethylcarbamoyl chloride

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

Conditions
ConditionsYield
With chlorosulphuric acid
With sulfur trioxide
Carbamidsaeure-methylester-N-sulfonsaeure-dimethylamid
89168-09-2

Carbamidsaeure-methylester-N-sulfonsaeure-dimethylamid

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

Conditions
ConditionsYield
With phosphorus pentachloride
C5H15N2O2S(1+)*Cl(1-)
29777-18-2

C5H15N2O2S(1+)*Cl(1-)

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

Conditions
ConditionsYield
at 60℃;
C2H6NO2S(1-)*Na(1+)

C2H6NO2S(1-)*Na(1+)

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

Conditions
ConditionsYield
With chlorine In tetrachloromethane
C2H6NO3S(1-)*Na(1+)
41955-27-5

C2H6NO3S(1-)*Na(1+)

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

Conditions
ConditionsYield
With trichlorophosphate In 1,2-dichloro-ethane at 80℃; for 18h;
antimony (V) pentachloride

antimony (V) pentachloride

N,N-dimethylammonium chloride
506-59-2

N,N-dimethylammonium chloride

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

Conditions
ConditionsYield
With sulfuryl dichloride In acetonitrile44.2 g (87%)
With sulfuryl dichloride In acetonitrile44.2 g (87%)
With sulfuryl dichloride In acetonitrile44.2 g (87%)
dipropylchloroborane
22086-53-9

dipropylchloroborane

tetramethylsulfamide
3768-63-6

tetramethylsulfamide

A

(dimethylamino)di-n-propylborane
13113-78-5

(dimethylamino)di-n-propylborane

B

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

dibutylchloroborane
1730-69-4

dibutylchloroborane

tetramethylsulfamide
3768-63-6

tetramethylsulfamide

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

4,4-ethylenedioxy-piperidine
177-11-7

4,4-ethylenedioxy-piperidine

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

N,N-dimethyl-1,4-dioxa-8-azaspiro[4.5]decane-8-sulfonamide
877796-41-3

N,N-dimethyl-1,4-dioxa-8-azaspiro[4.5]decane-8-sulfonamide

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃; for 1h;100%
dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

1-t-Butoxycarbonylpiperazine
57260-71-6

1-t-Butoxycarbonylpiperazine

(S)-6'-chloro-N-((R)-hept-6-en-3-ylsulfonyl)-5-((2-((S)-1-hydroxyallyl)-2-methylcyclobutyl)methyl)-3',4,4',5-tetrahydro-2H,2’H-spiro[benzo[b][1,4]oxazepine-3,1’-naphthalene]-7-carboxamide
253176-45-3

(S)-6'-chloro-N-((R)-hept-6-en-3-ylsulfonyl)-5-((2-((S)-1-hydroxyallyl)-2-methylcyclobutyl)methyl)-3',4,4',5-tetrahydro-2H,2’H-spiro[benzo[b][1,4]oxazepine-3,1’-naphthalene]-7-carboxamide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 24h; Inert atmosphere;100%
With triethylamine In dichloromethane at 20℃; for 12h;92%
With triethylamine at 0 - 20℃; for 4h; Inert atmosphere;89%
dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

1-t-Butoxycarbonylpiperazine
57260-71-6

1-t-Butoxycarbonylpiperazine

piperazine-1-sulfonic acid dimethylamide
98961-97-8

piperazine-1-sulfonic acid dimethylamide

Conditions
ConditionsYield
Stage #1: dimethylamino sulfonyl chloride; 1-t-Butoxycarbonylpiperazine With triethylamine In tetrahydrofuran at 0℃; for 1h;
Stage #2: With trifluoroacetic acid In dichloromethane at 20℃; for 48h;
Stage #3: With sodium hydroxide In dichloromethane; water
100%
N,N-diethyl-4-[7-hydroxy-6-methoxy-2-(trifluoroacetyl)-1,2,3,4-tetrahydroisoquinolin-1-yl]benzamide
857252-49-4

N,N-diethyl-4-[7-hydroxy-6-methoxy-2-(trifluoroacetyl)-1,2,3,4-tetrahydroisoquinolin-1-yl]benzamide

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

1-{4-[(diethylamino)carbonyl]phenyl}-6-methoxy-2-(trifluoroacetyl)-1,2,3,4-tetrahydroisoquinolin-7-yl dimethylsulfamate
857252-50-7

1-{4-[(diethylamino)carbonyl]phenyl}-6-methoxy-2-(trifluoroacetyl)-1,2,3,4-tetrahydroisoquinolin-7-yl dimethylsulfamate

Conditions
ConditionsYield
With triethylamine In dichloromethane at 0 - 20℃; for 22h;100%
dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

(2S,4S)-2-aminomethyl-1-p-methoxybenzyloxycarbonyl-4-tritylthiopyrrolidine
148016-92-6

(2S,4S)-2-aminomethyl-1-p-methoxybenzyloxycarbonyl-4-tritylthiopyrrolidine

(2S,4S)-1-p-methoxybenzyloxycarbonyl-2-N,N-dimethylsulfamoylaminomethyl-4-tritylthiopyrrolidine

(2S,4S)-1-p-methoxybenzyloxycarbonyl-2-N,N-dimethylsulfamoylaminomethyl-4-tritylthiopyrrolidine

Conditions
ConditionsYield
With triethylamine In dichloromethane100%
2-fluorophenol
367-12-4

2-fluorophenol

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

C8H10FNO3S
1201594-21-9

C8H10FNO3S

Conditions
ConditionsYield
Stage #1: 2-fluorophenol With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0 - 23℃; for 0.166667h;
Stage #2: dimethylamino sulfonyl chloride In 1,2-dimethoxyethane at 23℃; for 11h;
100%
salicylonitrile
611-20-1

salicylonitrile

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

C9H10N2O3S
1263387-24-1

C9H10N2O3S

Conditions
ConditionsYield
Stage #1: salicylonitrile With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0℃; for 0.166667h;
Stage #2: dimethylamino sulfonyl chloride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 11h;
100%
4-(3-(4-methoxyphenyl)-1H-indol-2-yl)-3,5-dimethylisoxazole
1288963-67-6

4-(3-(4-methoxyphenyl)-1H-indol-2-yl)-3,5-dimethylisoxazole

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

2-(3,5-dimethylisoxazol-4-yl)-3-(4-methoxyphenyl)-N,N-dimethyl-1H-indole-1-sulfonamide
1288963-72-3

2-(3,5-dimethylisoxazol-4-yl)-3-(4-methoxyphenyl)-N,N-dimethyl-1H-indole-1-sulfonamide

Conditions
ConditionsYield
Stage #1: 4-(3-(4-methoxyphenyl)-1H-indol-2-yl)-3,5-dimethylisoxazole With sodium hydride In n-heptane; N,N-dimethyl-formamide at 0 - 20℃; for 0.5h; Inert atmosphere;
Stage #2: dimethylamino sulfonyl chloride In n-heptane; N,N-dimethyl-formamide at 0 - 20℃; for 2h;
100%
Stage #1: 4-(3-(4-methoxyphenyl)-1H-indol-2-yl)-3,5-dimethylisoxazole With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 0.5h; Inert atmosphere;
Stage #2: dimethylamino sulfonyl chloride In N,N-dimethyl-formamide at 0 - 20℃; for 2h;
Stage #3: With water In N,N-dimethyl-formamide
100%
2-(3-amino-phenyl)-3,3-dimethyl-1,2,3,4-tetrahydro-quinoline-6-carboxylic acid ethyl ester
1343453-37-1

2-(3-amino-phenyl)-3,3-dimethyl-1,2,3,4-tetrahydro-quinoline-6-carboxylic acid ethyl ester

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

ethyl 2-(3-(N,N-dimethylsulfamoylamino)phenyl)-3,3-dimethyl-1,2,3,4-tetrahydroquinoline-6-carboxylate
1343454-35-2

ethyl 2-(3-(N,N-dimethylsulfamoylamino)phenyl)-3,3-dimethyl-1,2,3,4-tetrahydroquinoline-6-carboxylate

Conditions
ConditionsYield
With pyridine In dichloromethane at 0 - 25℃; for 16h;100%
With pyridine In dichloromethane at 0 - 25℃; for 16h;
3-methoxy-4-hydroxybenzonitrile
4421-08-3

3-methoxy-4-hydroxybenzonitrile

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

4-cyano-2-methoxyphenyl N,N-dimethylsulfamate
1432739-31-5

4-cyano-2-methoxyphenyl N,N-dimethylsulfamate

Conditions
ConditionsYield
Stage #1: 3-methoxy-4-hydroxybenzonitrile With dmap; triethylamine In dichloromethane at 20℃; for 0.166667h;
Stage #2: dimethylamino sulfonyl chloride In dichloromethane at 20℃; for 16h;
100%
4-chloro-phenol
106-48-9

4-chloro-phenol

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

4-chlorophenyl N,N-dimethylsulfamate
1135-05-3

4-chlorophenyl N,N-dimethylsulfamate

Conditions
ConditionsYield
Stage #1: 4-chloro-phenol With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 0.166667h;
Stage #2: dimethylamino sulfonyl chloride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 16h;
100%
Stage #1: 4-chloro-phenol With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 10h;
Stage #2: dimethylamino sulfonyl chloride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃;
83%
2,4-dichloro-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidine hydrochloride

2,4-dichloro-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidine hydrochloride

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

2,4-dichloro-N,N-dimethyl-5,8-dihydropyrido[3,4-d]pyrimidine-7(6H)-sulfonamide

2,4-dichloro-N,N-dimethyl-5,8-dihydropyrido[3,4-d]pyrimidine-7(6H)-sulfonamide

Conditions
ConditionsYield
Stage #1: 2,4-dichloro-5,6,7,8-tetrahydropyrido[3,4-d]pyrimidine hydrochloride With triethylamine In dichloromethane
Stage #2: dimethylamino sulfonyl chloride In dichloromethane
100%
NH-pyrazole
288-13-1

NH-pyrazole

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

N,N-dimethyl-1H-pyrazole-1-sulfonamide
133228-21-4

N,N-dimethyl-1H-pyrazole-1-sulfonamide

Conditions
ConditionsYield
Stage #1: NH-pyrazole With sodium hydride In tetrahydrofuran at 20℃; for 1h;
Stage #2: dimethylamino sulfonyl chloride In tetrahydrofuran for 1.5h;
99%
Stage #1: NH-pyrazole With sodium hydride In tetrahydrofuran; mineral oil at 0 - 20℃; for 0.5h; Inert atmosphere;
Stage #2: dimethylamino sulfonyl chloride In tetrahydrofuran; mineral oil at 0 - 20℃; for 0.5h; Inert atmosphere;
99%
With sodium hydride In tetrahydrofuran; mineral oil for 1.33333h; Inert atmosphere;91%
methoxybenzene
100-66-3

methoxybenzene

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

N,N-dimethyl-4-methoxybenzenesulfonamide
59907-37-8

N,N-dimethyl-4-methoxybenzenesulfonamide

Conditions
ConditionsYield
indium(III) triflate In 1,2-dichloro-ethane at 100℃; for 24h;99%
4-hydroxy-benzaldehyde
123-08-0

4-hydroxy-benzaldehyde

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

4-formylphenyl N,N-dimethylsulfamate

4-formylphenyl N,N-dimethylsulfamate

Conditions
ConditionsYield
With N,N-dimethyl-cyclohexanamine at 90 - 95℃; for 3h;99%
With N-ethyl-N,N-diisopropylamine at 90℃; for 2.5h;
4-Fluorophenol

4-Fluorophenol

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

4-fluorophenyl N,N-dimethylsulfamate
1259092-05-1

4-fluorophenyl N,N-dimethylsulfamate

Conditions
ConditionsYield
Stage #1: 4-Fluorophenol With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 0.166667h;
Stage #2: dimethylamino sulfonyl chloride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 16h;
99%
Stage #1: 4-Fluorophenol With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 0.25h; Inert atmosphere;
Stage #2: dimethylamino sulfonyl chloride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; Inert atmosphere;
91%
With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 11h; Inert atmosphere;
Stage #1: 4-Fluorophenol With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 0.166667h;
Stage #2: dimethylamino sulfonyl chloride In 1,2-dimethoxyethane; mineral oil at 0 - 20℃; for 12h;
4-ethoxycarbonylpyrazole
37622-90-5

4-ethoxycarbonylpyrazole

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

ethyl 1-(N,N-dimethylsulfamoyl)-1H-pyrazole-4-carboxylate

ethyl 1-(N,N-dimethylsulfamoyl)-1H-pyrazole-4-carboxylate

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane In acetonitrile for 1h; Inert atmosphere;99%
Stage #1: 4-ethoxycarbonylpyrazole With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 0.333333h; Inert atmosphere;
Stage #2: dimethylamino sulfonyl chloride In tetrahydrofuran; mineral oil at 25℃; for 22h; Inert atmosphere;
91%
methyl 3-(acetylamino)-1H-pyrazole-5-carboxylate
1202657-29-1

methyl 3-(acetylamino)-1H-pyrazole-5-carboxylate

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

C9H14N4O5S

C9H14N4O5S

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane In acetonitrile at 0 - 20℃; for 18h;99%
C17H19NO4

C17H19NO4

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

C23H34N4O10S3

C23H34N4O10S3

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃; for 10h;98.2%
methylamine
74-89-5

methylamine

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

N,N,N′-trimethylsulfamide
76820-42-3

N,N,N′-trimethylsulfamide

Conditions
ConditionsYield
In tetrahydrofuran98%
With potassium carbonate In tetrahydrofuran; dichloromethane at 0 - 25℃; for 2h;97%
In water; benzene at 50℃; for 5h;87%
With toluene
dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

N,N-dimethylsulfamide
3984-14-3

N,N-dimethylsulfamide

Conditions
ConditionsYield
With ammonia In methanol at 60℃; for 16h; Sealed tube;98%
With ammonium hydroxide at 0℃; for 3h;94%
With ammonium hydroxide at 0℃; ice-bath;76%
1H-imidazole
288-32-4

1H-imidazole

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

N,N-dimethyl-1H-imidazole-1-sulfonamide
78162-58-0

N,N-dimethyl-1H-imidazole-1-sulfonamide

Conditions
ConditionsYield
With triethylamine In toluene at 20℃; for 8h;98%
With triethylamine In benzene for 16h; Ambient temperature;95%
With triethylamine In diethyl ether at 20℃; for 16h;94.75%
1,6-anhydro-3,4-O-isopropylidene-β-D-galactopyranose
17073-95-9

1,6-anhydro-3,4-O-isopropylidene-β-D-galactopyranose

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

1,6-anhydro-2-O-(N,N-dimethylsulfamoyl)-3,4-O-isopropylidene-β-D-talopyranose
98815-77-1

1,6-anhydro-2-O-(N,N-dimethylsulfamoyl)-3,4-O-isopropylidene-β-D-talopyranose

Conditions
ConditionsYield
With 1H-imidazole; sodium hydride In tetrahydrofuran for 2h; Heating;98%
α-naphthol
90-15-3

α-naphthol

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

naphthalen-1-yl N,N-dimethylsulfamate
1144-13-4

naphthalen-1-yl N,N-dimethylsulfamate

Conditions
ConditionsYield
With sodium hydride In 1,2-dimethoxyethane at 23℃; for 17h; Inert atmosphere;98%
Stage #1: α-naphthol With sodium hydride In 1,2-dimethoxyethane; mineral oil at 0 - 23℃; for 0.166667h;
Stage #2: dimethylamino sulfonyl chloride In 1,2-dimethoxyethane; mineral oil at 23℃; for 11h;
95%
With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride In benzene at 50℃; for 6h;94%
4(5)-(4-tolyl)-1H-imidazole
670-91-7

4(5)-(4-tolyl)-1H-imidazole

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

1-(dimethylsulfamoyl)-5-p-tolylimidazole

1-(dimethylsulfamoyl)-5-p-tolylimidazole

Conditions
ConditionsYield
With potassium carbonate In ethyl acetate at 77℃; for 6h; Temperature;98%
C17H20N6

C17H20N6

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

C21H30N8O4S2

C21H30N8O4S2

Conditions
ConditionsYield
Stage #1: C17H20N6 With sodium hydroxide In N,N-dimethyl-formamide for 0.5h; Cooling;
Stage #2: dimethylamino sulfonyl chloride In N,N-dimethyl-formamide at 220℃; for 4h; Autoclave;
97.6%
4-iodoimidazole
71759-89-2

4-iodoimidazole

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

4-iodo-N,N-dimethyl-1H-imidazole-1-sulfonamide
135773-25-0

4-iodo-N,N-dimethyl-1H-imidazole-1-sulfonamide

Conditions
ConditionsYield
Stage #1: 4-iodoimidazole; dimethylamino sulfonyl chloride With sodium hydroxide In tetrahydrofuran at 8 - 20℃;
Stage #2: In n-heptane at 70℃; for 4h;
97.3%
With triethylamine In acetonitrile at 20℃; for 2h;80%
With triethylamine In dichloromethane for 60h; Heating;60%
With triethylamine In dichloromethane at 20℃; for 26h; Inert atmosphere;58%
2-methyl-propan-1-ol
78-83-1

2-methyl-propan-1-ol

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

isobutyl N,N-dimethylsulfamate
66950-72-9

isobutyl N,N-dimethylsulfamate

Conditions
ConditionsYield
With sodium hydride In 1,2-dimethoxyethane97%
(+/-)-(1S*,6S*,8R*,9R*,10S*,11S*)-2,2-Dimethoxy-10,11-epoxy-6-methyl-12-oxatricyclo<6.3.1.01,6>dodecan-9-ol

(+/-)-(1S*,6S*,8R*,9R*,10S*,11S*)-2,2-Dimethoxy-10,11-epoxy-6-methyl-12-oxatricyclo<6.3.1.01,6>dodecan-9-ol

dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

C16H27NO7S

C16H27NO7S

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran 1.) r.t., 5 min, 2.) r.t., 1 h;97%
dimethylamino sulfonyl chloride
13360-57-1

dimethylamino sulfonyl chloride

3,4-bis(trimethylsilyl)-1H-pyrrole
195820-65-6

3,4-bis(trimethylsilyl)-1H-pyrrole

N-N-dimethyl 3,4-bis(trimethylsilyl)-1H-pyrrole-1-sulfonamide
278167-17-2

N-N-dimethyl 3,4-bis(trimethylsilyl)-1H-pyrrole-1-sulfonamide

Conditions
ConditionsYield
Stage #1: 3,4-bis(trimethylsilyl)-1H-pyrrole With sodium hydride In N,N-dimethyl-formamide at 0℃; for 2h; Metallation;
Stage #2: dimethylamino sulfonyl chloride In N,N-dimethyl-formamide at 0 - 20℃; for 2h; Substitution; Further stages.;
97%
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