5,10-bis(pentafluorophenyl)tripyrrane

Base Information

• Chemical Name: 5,10-bis(pentafluorophenyl)tripyrrane
• CAS No.: 292164-60-4
• Molecular Formula: C₂₆H₁₃F₁₀N₃
• Molecular Weight: 557.393
• Mol file: 292164-60-4.mol

Synonyms:5,10-bis(pentafluorophenyl)tripyrrane

Chemical Property of 5,10-bis(pentafluorophenyl)tripyrrane

Chemical Property:

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Technology Process of 5,10-bis(pentafluorophenyl)tripyrrane

There total 3 articles about 5,10-bis(pentafluorophenyl)tripyrrane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

pyrrole (109-97-7,30604-81-0) + perfluorobenzaldehyde (653-37-2) → 5-(pentafluorophenyl)dipyrromethane (167482-91-9) + 5,10-bis(pentafluorophenyl)tripyrrane (292164-60-4)

Guidance literature:

With trifluoroacetic acid; at 20 ℃; for 0.0833333h;

DOI:10.1016/S0040-4039(00)00672-9

Reference yield: 18.4%

pyrrole (109-97-7,30604-81-0) + perfluorobenzaldehyde (653-37-2) → 5,10-bis(pentafluorophenyl)tripyrrane (292164-60-4)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 15 - 20 ℃; for 0.5h;

DOI:10.1002/ejoc.201500276

Reference yield:

C74H54F20N4O4Sn2 → 5,10-bis(pentafluorophenyl)tripyrrane (292164-60-4)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; methanol; for 0.5h; Darkness;

DOI:10.1002/chem.201900819

upstream raw materials:

pyrrole

perfluorobenzaldehyde

Downstream raw materials:

tetrakis(pentafluorophenyl)porphyrin