(S)-4-benzyloxy-2-{2-[benzyloxycarbonyl-(2-carboxy-ethyl)-amino]-ethylamino}-butyric acid methyl ester; hydrochloride

Base Information

Chemical Name:(S)-4-benzyloxy-2-{2-[benzyloxycarbonyl-(2-carboxy-ethyl)-amino]-ethylamino}-butyric acid methyl ester; hydrochloride
CAS No.:1205542-43-3
Molecular Formula:C₂₅H₃₂N₂O₇*ClH
Molecular Weight:508.999
Hs Code.:

Synonyms:(S)-4-benzyloxy-2-{2-[benzyloxycarbonyl-(2-carboxy-ethyl)-amino]-ethylamino}-butyric acid methyl ester; hydrochloride

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Chemical Property of (S)-4-benzyloxy-2-{2-[benzyloxycarbonyl-(2-carboxy-ethyl)-amino]-ethylamino}-butyric acid methyl ester; hydrochloride

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Technology Process of (S)-4-benzyloxy-2-{2-[benzyloxycarbonyl-(2-carboxy-ethyl)-amino]-ethylamino}-butyric acid methyl ester; hydrochloride

There total 6 articles about (S)-4-benzyloxy-2-{2-[benzyloxycarbonyl-(2-carboxy-ethyl)-amino]-ethylamino}-butyric acid methyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1205542-42-2
(S)-4-benzyloxy-2-{2-[benzyloxycarbonyl-(2-tert-butoxycarbonyl-ethyl)-amino]-ethylamino}-butyric acid methyl ester

: 1205542-43-3
(S)-4-benzyloxy-2-{2-[benzyloxycarbonyl-(2-carboxy-ethyl)-amino]-ethylamino}-butyric acid methyl ester; hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; water; at 20 ℃; for 12h;

Reference yield:

: 13139-17-8
N-(Benzyloxycarbonyloxy)succinimide

: 1205542-43-3
(S)-4-benzyloxy-2-{2-[benzyloxycarbonyl-(2-carboxy-ethyl)-amino]-ethylamino}-butyric acid methyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1.1: 18 h / 0 - 30 °C

1.2: 3 h / 0 - 20 °C

2.1: triethylamine; oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -60 - -50 °C

3.1: triethylamine; acetic acid; borane pyridine / ethanol; 1,2-dichloro-ethane / 1.25 h / 20 °C

4.1: hydrogenchloride; water / 1,4-dioxane / 12 h / 10 - 20 °C

With hydrogenchloride; oxalyl dichloride; borane pyridine; water; acetic acid; dimethyl sulfoxide; triethylamine; In 1,4-dioxane; ethanol; dichloromethane; 1,2-dichloro-ethane;

Reference yield:

: 1205542-41-1
3-[benzyloxycarbonyl-(2-oxo-ethyl)-amino]-propionic acid tert-butyl ester

: 1205542-43-3
(S)-4-benzyloxy-2-{2-[benzyloxycarbonyl-(2-carboxy-ethyl)-amino]-ethylamino}-butyric acid methyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine; acetic acid; borane pyridine / ethanol; 1,2-dichloro-ethane / 1.25 h / 20 °C

2: hydrogenchloride; water / 1,4-dioxane / 12 h / 10 - 20 °C

With hydrogenchloride; borane pyridine; water; acetic acid; triethylamine; In 1,4-dioxane; ethanol; 1,2-dichloro-ethane;