dimethylthexylsilyl O-(2-O-acetyl-3-O-benzyl-β-D-glucopyranosyl)-(1->4)-O-2-azido-3-O-benzyl-6-O-levulinoyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:dimethylthexylsilyl O-(2-O-acetyl-3-O-benzyl-β-D-glucopyranosyl)-(1->4)-O-2-azido-3-O-benzyl-6-O-levulinoyl-2-deoxy-β-D-glucopyranoside
CAS No.:1198157-07-1
Molecular Formula:C₄₁H₅₉N₃O₁₃Si
Molecular Weight:830.017
Hs Code.:

Synonyms:dimethylthexylsilyl O-(2-O-acetyl-3-O-benzyl-β-D-glucopyranosyl)-(1->4)-O-2-azido-3-O-benzyl-6-O-levulinoyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of dimethylthexylsilyl O-(2-O-acetyl-3-O-benzyl-β-D-glucopyranosyl)-(1->4)-O-2-azido-3-O-benzyl-6-O-levulinoyl-2-deoxy-β-D-glucopyranoside

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Technology Process of dimethylthexylsilyl O-(2-O-acetyl-3-O-benzyl-β-D-glucopyranosyl)-(1->4)-O-2-azido-3-O-benzyl-6-O-levulinoyl-2-deoxy-β-D-glucopyranoside

There total 4 articles about dimethylthexylsilyl O-(2-O-acetyl-3-O-benzyl-β-D-glucopyranosyl)-(1->4)-O-2-azido-3-O-benzyl-6-O-levulinoyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1198156-17-0
dimethylthexylsilyl O-(2-O-acetyl-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranosyl)-(1->4)-O-2-azido-3-O-benzyl-6-O-levulinoyl-2-deoxy-β-D-glucopyranoside

: 1198157-07-1
dimethylthexylsilyl O-(2-O-acetyl-3-O-benzyl-β-D-glucopyranosyl)-(1->4)-O-2-azido-3-O-benzyl-6-O-levulinoyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: With water; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1021/ja907358k

Reference yield: 85.0%

: 1198157-07-1
dimethylthexylsilyl O-(2-O-acetyl-3-O-benzyl-β-D-glucopyranosyl)-(1->4)-O-2-azido-3-O-benzyl-6-O-levulinoyl-2-deoxy-β-D-glucopyranoside

Guidance literature:

Reference yield:

: C₂₄H₂₈O₆S

: 1198157-07-1
dimethylthexylsilyl O-(2-O-acetyl-3-O-benzyl-β-D-glucopyranosyl)-(1->4)-O-2-azido-3-O-benzyl-6-O-levulinoyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / 0 °C / Molecular sieve

2: trifluoroacetic acid / dichloromethane; water / 0.5 h

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; trifluoroacetic acid; In dichloromethane; water;
DOI:10.1021/acs.joc.0c01881