2-[1-(3-chloropyridine-2-yl)-3-bromo-1H-pyrazole-5-yl]-6-iodo-8-methyl-4H-3,1-benzoxazine-4-one

Base Information

Chemical Name:2-[1-(3-chloropyridine-2-yl)-3-bromo-1H-pyrazole-5-yl]-6-iodo-8-methyl-4H-3,1-benzoxazine-4-one
CAS No.:736995-63-4
Molecular Formula:C₁₇H₉BrClIN₄O₂
Molecular Weight:543.546
Hs Code.:

Synonyms:2-[1-(3-chloropyridine-2-yl)-3-bromo-1H-pyrazole-5-yl]-6-iodo-8-methyl-4H-3,1-benzoxazine-4-one

Suppliers and Price of 2-[1-(3-chloropyridine-2-yl)-3-bromo-1H-pyrazole-5-yl]-6-iodo-8-methyl-4H-3,1-benzoxazine-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Matrix Scientific
2-[5-Bromo-2-(3-chloro-pyridin-2-yl)-2H-pyrazol-3-yl]-6-iodo-8-methyl-benzo[d][1,3]oxazin-4-one 95%+
1g
$ 1790.00

Matrix Scientific
2-[5-Bromo-2-(3-chloro-pyridin-2-yl)-2H-pyrazol-3-yl]-6-iodo-8-methyl-benzo[d][1,3]oxazin-4-one 95%+
500mg
$ 950.00

Advanced Chemicals Intermediatesced Chemicals Intermediates
2-[5-Bromo-2-(3-chloro-pyridin-2-yl)-2H-pyrazol-3-yl]-6-iodo-8-methyl-benzo[d][1,3]oxazin-4-one 95%+
1g
$ 710.50

Acints
2-[5-Bromo-2-(3-chloro-pyridin-2-yl)-2H-pyrazol-3-yl]-6-iodo-8-methyl-benzo[d][1,3]oxazin-4-one 95%+
5g
$ 2167.75

Acints
2-[5-Bromo-2-(3-chloro-pyridin-2-yl)-2H-pyrazol-3-yl]-6-iodo-8-methyl-benzo[d][1,3]oxazin-4-one 95%+
1g
$ 710.50

Acints
2-[5-Bromo-2-(3-chloro-pyridin-2-yl)-2H-pyrazol-3-yl]-6-iodo-8-methyl-benzo[d][1,3]oxazin-4-one 95%+
500mg
$ 384.25

Total 1 raw suppliers

Chemical Property of 2-[1-(3-chloropyridine-2-yl)-3-bromo-1H-pyrazole-5-yl]-6-iodo-8-methyl-4H-3,1-benzoxazine-4-one

Chemical Property:

Purity/Quality:

95%-98% ^*data from raw suppliers

2-[5-Bromo-2-(3-chloro-pyridin-2-yl)-2H-pyrazol-3-yl]-6-iodo-8-methyl-benzo[d][1,3]oxazin-4-one 95%+ ^*data from reagent suppliers

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Technology Process of 2-[1-(3-chloropyridine-2-yl)-3-bromo-1H-pyrazole-5-yl]-6-iodo-8-methyl-4H-3,1-benzoxazine-4-one

There total 2 articles about 2-[1-(3-chloropyridine-2-yl)-3-bromo-1H-pyrazole-5-yl]-6-iodo-8-methyl-4H-3,1-benzoxazine-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.9%

: 500011-86-9
3-bromo-1-(3-chloro-2-pyridinyl)-1H-pyrazole-5-carboxylic acid

: 108857-24-5
2-amino-5-iodo-3-methylbenzoic acid

: 736995-63-4
2-[1-(3-chloropyridine-2-yl)-3-bromo-1H-pyrazole-5-yl]-6-iodo-8-methyl-4H-3,1-benzoxazine-4-one

Guidance literature:: With methanesulfonyl chloride; In acetonitrile; at -8 - 15 ℃; for 3.5h;

Reference yield:

: 4389-45-1
3-methylantranilic acid

: 736995-63-4
2-[1-(3-chloropyridine-2-yl)-3-bromo-1H-pyrazole-5-yl]-6-iodo-8-methyl-4H-3,1-benzoxazine-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: iodine; dipotassium peroxodisulfate / tetrachloromethane / 6 h / 77 °C

2: methanesulfonyl chloride; triethylamine / tetrahydrofuran / 3 h / -8 - 15 °C

With dipotassium peroxodisulfate; iodine; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; tetrachloromethane;