methyl 4-[({2-[(tert-butoxycarbonyl)(d³-methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate

Base Information

• Chemical Name: methyl 4-[({2-[(tert-butoxycarbonyl)(d³-methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate
• CAS No.: 330798-30-6
• Molecular Formula: C₁₆H₂₃N₃O₈S
• Molecular Weight: 420.416

Synonyms:methyl 4-[({2-[(tert-butoxycarbonyl)(d³-methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate

Chemical Property of methyl 4-[({2-[(tert-butoxycarbonyl)(d³-methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate

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Technology Process of methyl 4-[({2-[(tert-butoxycarbonyl)(d³-methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate

There total 1 articles about methyl 4-[({2-[(tert-butoxycarbonyl)(d³-methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

4-chlorosulfonyl-3-nitrobenzoic acid methyl ester (162010-78-8) + C8H15(2)H3N2O2 → methyl 4-[({2-[(tert-butoxycarbonyl)(d3-methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate (330798-30-6)

Guidance literature:

With diisopropylamine; In dichloromethane; at 20 ℃; for 6h;

DOI:10.1021/ol006751n

Reference yield: 86.0%

3-(9-anthracenyl)propyl bromide (22756-32-7) + methyl 4-[({2-[(tert-butoxycarbonyl)(d3-methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate (330798-30-6) → methyl 4-[([3-(9-anthryl)propyl]{2-[(tert-butoxycarbonyl)(d3-methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate (330798-32-8)

Guidance literature:

With PS-BEMP; In N,N-dimethyl-formamide; at 20 ℃; for 14h;

DOI:10.1021/ol006751n

Reference yield:

methyl 4-[({2-[(tert-butoxycarbonyl)(d3-methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate (330798-30-6) → C32H32(2)H3N3O8S

Guidance literature:

Multi-step reaction with 2 steps

1: 86 percent / PS-BEMP / dimethylformamide / 14 h / 20 °C

2: aq. NaOH / tetrahydrofuran; methanol / 3 h / 20 °C

With sodium hydroxide; PS-BEMP; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;

DOI:10.1021/ol006751n

upstream raw materials:

4-chlorosulfonyl-3-nitrobenzoic acid methyl ester

Downstream raw materials:

methyl 4-[([3-(9-anthryl)propyl]{2-[(tert-butoxycarbonyl)(d³-methyl)amino]ethyl}amino)sulphonyl]-3-nitrobenzoate

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