3-[3-(2-chloro-1H-benzoimidazol-4-yl)thioureido]-4-isopropoxy-benzamide

Base Information

Chemical Name:3-[3-(2-chloro-1H-benzoimidazol-4-yl)thioureido]-4-isopropoxy-benzamide
CAS No.:1378078-73-9
Molecular Formula:C₁₈H₁₈ClN₅O₂S
Molecular Weight:403.892
Hs Code.:

Synonyms:3-[3-(2-chloro-1H-benzoimidazol-4-yl)thioureido]-4-isopropoxy-benzamide

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Chemical Property of 3-[3-(2-chloro-1H-benzoimidazol-4-yl)thioureido]-4-isopropoxy-benzamide

Chemical Property:

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Technology Process of 3-[3-(2-chloro-1H-benzoimidazol-4-yl)thioureido]-4-isopropoxy-benzamide

There total 6 articles about 3-[3-(2-chloro-1H-benzoimidazol-4-yl)thioureido]-4-isopropoxy-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1377581-87-7
4-Isopropoxy-3-isothiocyanato-benzamide

: 1378078-31-9
2-chloro-1H-1,3-benzodiazol-4-amine

: 1378078-73-9
3-[3-(2-chloro-1H-benzoimidazol-4-yl)thioureido]-4-isopropoxy-benzamide

Guidance literature:: In dimethyl sulfoxide; at 65 ℃; for 5h; Inert atmosphere;

Reference yield:

: 400-94-2
4-fluoro-3-nitrobenzoyl chloride

: 1378078-73-9
3-[3-(2-chloro-1H-benzoimidazol-4-yl)thioureido]-4-isopropoxy-benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: ammonium hydroxide / water; tetrahydrofuran / 0.58 h / 0 °C

2: potassium hexamethylsilazane / toluene; tetrahydrofuran / 0 - 23 °C

3: sodium tetrahydroborate; nickel(II) chloride hexahydrate / methanol / 1 h / 0 - 23 °C

4: sodium hydrogencarbonate / chloroform; water / 3.17 h / 20 °C

5: dimethyl sulfoxide / 5 h / 65 °C / Inert atmosphere

With ammonium hydroxide; sodium tetrahydroborate; nickel(II) chloride hexahydrate; potassium hexamethylsilazane; sodium hydrogencarbonate; In tetrahydrofuran; methanol; chloroform; water; dimethyl sulfoxide; toluene;

Reference yield:

: 349-02-0
4-fluoro-3-nitrobenzamide

: 1378078-73-9
3-[3-(2-chloro-1H-benzoimidazol-4-yl)thioureido]-4-isopropoxy-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hexamethylsilazane / toluene; tetrahydrofuran / 0 - 23 °C

2: sodium tetrahydroborate; nickel(II) chloride hexahydrate / methanol / 1 h / 0 - 23 °C

3: sodium hydrogencarbonate / chloroform; water / 3.17 h / 20 °C

4: dimethyl sulfoxide / 5 h / 65 °C / Inert atmosphere

With sodium tetrahydroborate; nickel(II) chloride hexahydrate; potassium hexamethylsilazane; sodium hydrogencarbonate; In tetrahydrofuran; methanol; chloroform; water; dimethyl sulfoxide; toluene;