C₂₄H₃₁BrO₆

Base Information

• Chemical Name: C₂₄H₃₁BrO₆
• CAS No.: 715654-70-9
• Molecular Formula: C₂₄H₃₁BrO₆
• Molecular Weight: 495.411
• Mol file: 715654-70-9.mol

Synonyms:C₂₄H₃₁BrO₆

Chemical Property of C₂₄H₃₁BrO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₄H₃₁BrO₆

There total 7 articles about C₂₄H₃₁BrO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C24H32O6 (259814-29-4) → C24H31BrO6 (715654-70-9)

Guidance literature:

With N-Bromosuccinimide; calcium carbonate; In tetrahydrofuran; at 0 ℃;

DOI:10.1016/S0040-4039(01)02203-1

Reference yield:

santonin (481-06-1) → C24H31BrO6 (715654-70-9)

Guidance literature:

Multi-step reaction with 7 steps

1.1: H₂ / Raney Ni / benzene

1.2: 53 percent / PTS / toluene

2.1: 68 percent / m-CPBA / CH₂Cl₂

3.1: 83 percent / NaOMe / methanol

4.1: 95 percent / LiAlH₄ / tetrahydrofuran / -78 - 20 °C

5.1: 70 percent / ZnCl₂ / 20 °C

6.1: 75 percent / SeO₂; t-BuO₂H

7.1: 95 percent / NBS; CaCO₃ / tetrahydrofuran / 0 °C

With tert.-butylhydroperoxide; N-Bromosuccinimide; lithium aluminium tetrahydride; selenium(IV) oxide; hydrogen; sodium methylate; 3-chloro-benzenecarboperoxoic acid; calcium carbonate; zinc(II) chloride; nickel; In tetrahydrofuran; methanol; dichloromethane; benzene;

DOI:10.1016/S0040-4039(01)02203-1

Reference yield:

3,3-ethylenedioxy-5α-hydroxy-4α,6β-uedesm-7(11)-en-6,13-olide (215245-11-7) → C24H31BrO6 (715654-70-9)

Guidance literature:

Multi-step reaction with 4 steps

1: 95 percent / LiAlH₄ / tetrahydrofuran / -78 - 20 °C

2: 70 percent / ZnCl₂ / 20 °C

3: 75 percent / SeO₂; t-BuO₂H

4: 95 percent / NBS; CaCO₃ / tetrahydrofuran / 0 °C

With tert.-butylhydroperoxide; N-Bromosuccinimide; lithium aluminium tetrahydride; selenium(IV) oxide; calcium carbonate; zinc(II) chloride; In tetrahydrofuran;

DOI:10.1016/S0040-4039(01)02203-1

upstream raw materials:

C₂₄H₃₂O₆

3,3-ethylenedioxy-5α-hydroxy-4α,6β-uedesm-7(11)-en-6,13-olide

3,3-ethylenedioxy-4,7α,11βH-eudesm-5-en-6,13-olide

C₁₇H₂₄O₅

Downstream raw materials:

C₂₄H₃₂O₇

C₂₄H₃₀O₅

C₂₄H₃₂O₆