5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-3,4,6-tri-O-benzyl-β-D-mannopyranoside

Base Information

• Chemical Name: 5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-3,4,6-tri-O-benzyl-β-D-mannopyranoside
• CAS No.: 1011529-43-3
• Molecular Formula: C₆₀H₆₂O₁₅
• Molecular Weight: 1023.14

Synonyms:5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-3,4,6-tri-O-benzyl-β-D-mannopyranoside

Chemical Property of 5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-3,4,6-tri-O-benzyl-β-D-mannopyranoside

Chemical Property:

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Technology Process of 5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-3,4,6-tri-O-benzyl-β-D-mannopyranoside

There total 1 articles about 5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-3,4,6-tri-O-benzyl-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

(2-methyl-5-tert-butylphenyl) 2,3,4-tri-O-benzoyl-1-thio-D-xylopyranoside + 5-methoxycarbonylpentyl 3,4,6-tri-O-benzyl-β-D-mannopyranoside (1011529-42-2) → 5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-3,4,6-tri-O-benzyl-β-D-mannopyranoside (1011529-43-3)

Guidance literature:

With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; In dichloromethane; at 20 ℃;

DOI:10.1016/j.tet.2007.11.002

Reference yield: 92.0%

5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-3,4,6-tri-O-benzyl-β-D-mannopyranoside (1011529-43-3) → 5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-β-D-mannopyranoside (1011529-45-5)

Guidance literature:

With methanol; hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃;

DOI:10.1016/j.tet.2007.11.002

upstream raw materials:

5-methoxycarbonylpentyl 3,4,6-tri-O-benzyl-β-D-mannopyranoside

Downstream raw materials:

5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-β-D-mannopyranoside

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