5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-β-D-mannopyranoside

Base Information

Chemical Name:5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-β-D-mannopyranoside
CAS No.:1011529-45-5
Molecular Formula:C₃₉H₄₄O₁₅
Molecular Weight:752.769
Hs Code.:

Synonyms:5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-β-D-mannopyranoside

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Chemical Property of 5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-β-D-mannopyranoside

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Technology Process of 5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-β-D-mannopyranoside

There total 1 articles about 5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1011529-43-3
5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-3,4,6-tri-O-benzyl-β-D-mannopyranoside

: 1011529-45-5
5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-β-D-mannopyranoside

Guidance literature:: With methanol; hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃;
DOI:10.1016/j.tet.2007.11.002

Reference yield: 89.0%

: 1011529-45-5
5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-β-D-mannopyranoside

: 1125-88-8
benzaldehyde dimethyl acetal

: 1276117-26-0
C₄₆H₄₈O₁₅

Guidance literature:: With camphor-10-sulfonic acid; In acetonitrile; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2010.12.001

Reference yield: 70.0%

: 1011529-45-5
5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-β-D-mannopyranoside

: 98-88-4
benzoyl chloride

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1011529-46-6
5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-3,4-di-O-benzoyl-6-O-tert-butyldimethylsilyl-β-D-mannopyranoside

Guidance literature:: 5-methoxycarbonylpentyl 2-O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-β-D-mannopyranoside; tert-butyldimethylsilyl chloride; With dmap; In pyridine; at 20 ℃;

benzoyl chloride; In pyridine; at 20 ℃; for 2h; Further stages.;
DOI:10.1016/j.tet.2007.11.002