tert-butyl 2-[2-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}-4-[2-(tert-butoxycarbonylamino)ethyl]phenoxy)ethoxy]ethylcarbamate

Base Information

Chemical Name:tert-butyl 2-[2-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}-4-[2-(tert-butoxycarbonylamino)ethyl]phenoxy)ethoxy]ethylcarbamate
CAS No.:1400565-41-4
Molecular Formula:C₃₁H₅₃N₃O₁₀
Molecular Weight:627.776
Hs Code.:

Synonyms:tert-butyl 2-[2-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}-4-[2-(tert-butoxycarbonylamino)ethyl]phenoxy)ethoxy]ethylcarbamate

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Chemical Property of tert-butyl 2-[2-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}-4-[2-(tert-butoxycarbonylamino)ethyl]phenoxy)ethoxy]ethylcarbamate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of tert-butyl 2-[2-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}-4-[2-(tert-butoxycarbonylamino)ethyl]phenoxy)ethoxy]ethylcarbamate

There total 2 articles about tert-butyl 2-[2-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}-4-[2-(tert-butoxycarbonylamino)ethyl]phenoxy)ethoxy]ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 192132-77-7
2-(2-(tert-butoxycarbonylamino)ethoxy)ethyl 4-methylbenzenesulfonate

: 37034-31-4
N-(tert-butoxycarbonyl)dopamine

: 1400565-41-4
tert-butyl 2-[2-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}-4-[2-(tert-butoxycarbonylamino)ethyl]phenoxy)ethoxy]ethylcarbamate

Guidance literature:: N-(tert-butoxycarbonyl)dopamine; With caesium carbonate; In methanol; at 45 ℃; for 0.5h; Inert atmosphere;

2-(2-(tert-butoxycarbonylamino)ethoxy)ethyl 4-methylbenzenesulfonate; In N,N-dimethyl-formamide; at 60 ℃; Inert atmosphere;
DOI:10.1055/s-0031-1290444

Reference yield:

: 139115-91-6
2-(2-tert-butyloxycarbonylaminoethoxy)ethanol

: 1400565-41-4
tert-butyl 2-[2-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}-4-[2-(tert-butoxycarbonylamino)ethyl]phenoxy)ethoxy]ethylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: dmap; triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere

2.1: caesium carbonate / methanol / 0.5 h / 45 °C / Inert atmosphere

2.2: 60 °C / Inert atmosphere

With dmap; caesium carbonate; triethylamine; In methanol; dichloromethane;
DOI:10.1055/s-0031-1290444

Reference yield:

: 1400565-41-4
tert-butyl 2-[2-(2-{2-[2-(tert-butoxycarbonylamino)ethoxy]ethoxy}-4-[2-(tert-butoxycarbonylamino)ethyl]phenoxy)ethoxy]ethylcarbamate

: 1400565-47-0
N,N'-({4-[2-(4-azido-2,3,5,6-tetrafluorobenzamido)ethyl]-1,2-phenylene}bis(oxyethane-2,1-diyloxyethane-2,1-diyl))bis(4-azido-2,3,5,6-tetrafluorobenzamide)

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 2 h / 20 °C

2: triethylamine / dichloromethane

With triethylamine; In dichloromethane;
DOI:10.1055/s-0031-1290444