1,3-Diphenyl-2-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-ylmethoxy)-[1,3,2]diazaphospholidine

Base Information

Chemical Name:1,3-Diphenyl-2-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-ylmethoxy)-[1,3,2]diazaphospholidine
CAS No.:85597-20-2
Molecular Formula:C₂₆H₃₃N₂O₆P
Molecular Weight:500.532
Hs Code.:

Synonyms:1,3-Diphenyl-2-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-ylmethoxy)-[1,3,2]diazaphospholidine

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Chemical Property of 1,3-Diphenyl-2-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-ylmethoxy)-[1,3,2]diazaphospholidine

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MSDS Files:: SDS file from LookChem

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Technology Process of 1,3-Diphenyl-2-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-ylmethoxy)-[1,3,2]diazaphospholidine

There total 2 articles about 1,3-Diphenyl-2-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-ylmethoxy)-[1,3,2]diazaphospholidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 81106-32-3
dimethylamino-2,N,N' diphenyl-1,3 diazaphospholane-1,3,2

: 4064-06-6
1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: 85597-20-2
1,3-Diphenyl-2-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-ylmethoxy)-[1,3,2]diazaphospholidine

Guidance literature:: In toluene; at 85 ℃;
DOI:10.1016/S0040-4039(00)85615-4

Reference yield:

: 150-61-8
N,N'-diphenylethylenediamine

: 85597-20-2
1,3-Diphenyl-2-((3aR,5R,5aS,8aS,8bR)-2,2,7,7-tetramethyl-tetrahydro-bis[1,3]dioxolo[4,5-b;4',5'-d]pyran-5-ylmethoxy)-[1,3,2]diazaphospholidine

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / toluene / 24 h / Heating

2: 70 percent / toluene / 85 °C

In toluene;
DOI:10.1016/S0040-4039(00)85615-4