N,N-dihexadecyl-N^α-tert-butoxycarbonyl-O-benzyl-L-glutamic acid α-amide

Base Information

Chemical Name:N,N-dihexadecyl-N^α-tert-butoxycarbonyl-O-benzyl-L-glutamic acid α-amide
CAS No.:748818-26-0
Molecular Formula:C₄₉H₈₈N₂O₅
Molecular Weight:785.248
Hs Code.:

N,N-dihexadecyl-N<sup>α</sup>-tert-butoxycarbonyl-O-benzyl-L-glutamic acid α-amide

Synonyms:N,N-dihexadecyl-N^α-tert-butoxycarbonyl-O-benzyl-L-glutamic acid α-amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-dihexadecyl-N^α-tert-butoxycarbonyl-O-benzyl-L-glutamic acid α-amide

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Technology Process of N,N-dihexadecyl-N^α-tert-butoxycarbonyl-O-benzyl-L-glutamic acid α-amide

There total 1 articles about N,N-dihexadecyl-N^α-tert-butoxycarbonyl-O-benzyl-L-glutamic acid α-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 16724-63-3
dihexadecylamine

: 13574-13-5
Boc-Glu(OBzl)-OH

: 748818-26-0
N,N-dihexadecyl-N^α-tert-butoxycarbonyl-O-benzyl-L-glutamic acid α-amide

Guidance literature:: Boc-Glu(OBzl)-OH; With dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 0.5h;

dihexadecylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/ja053226g

Reference yield:

: 748818-26-0
N,N-dihexadecyl-N^α-tert-butoxycarbonyl-O-benzyl-L-glutamic acid α-amide

: (S)-4-Amino-4-dihexadecylcarbamoyl-butyric acid benzyl ester

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1021/ja053226g

Reference yield:

: 748818-26-0
N,N-dihexadecyl-N^α-tert-butoxycarbonyl-O-benzyl-L-glutamic acid α-amide

: 864846-75-3
N,N-dihexadecyl-N^α-6-bromohexanoyl-O-benzyl-L-glutamic acid α-amide

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / CH₂Cl₂ / 2 h / 0 °C

2: 0.205 g / CH₂Cl₂ / 0 °C

With trifluoroacetic acid; In dichloromethane;
DOI:10.1021/ja053226g