2-((6-chloropyridin-3-yl)methoxy)-N-(3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)phenyl)benzamide

Base Information

Chemical Name:2-((6-chloropyridin-3-yl)methoxy)-N-(3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)phenyl)benzamide
CAS No.:1415750-46-7
Molecular Formula:C₂₁H₁₃Cl₃F₄N₂O₃
Molecular Weight:523.698
Hs Code.:

Synonyms:2-((6-chloropyridin-3-yl)methoxy)-N-(3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)phenyl)benzamide

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Chemical Property of 2-((6-chloropyridin-3-yl)methoxy)-N-(3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)phenyl)benzamide

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Technology Process of 2-((6-chloropyridin-3-yl)methoxy)-N-(3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)phenyl)benzamide

There total 5 articles about 2-((6-chloropyridin-3-yl)methoxy)-N-(3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)phenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 2-((6-chloropyridin-3-yl)methoxy)benzoyl chloride

: 104147-32-2
3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)benzeneamine

: 1415750-46-7
2-((6-chloropyridin-3-yl)methoxy)-N-(3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)phenyl)benzamide

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; Cooling with ice;
DOI:10.1007/s00044-012-0380-8

Reference yield:

: 69-72-7,25496-36-0,8052-31-1
salicylic acid

: 1415750-46-7
2-((6-chloropyridin-3-yl)methoxy)-N-(3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)phenyl)benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: sulfuric acid

2: potassium carbonate / acetonitrile

3: water; sodium hydroxide / methanol

4: thionyl chloride / toluene / 2 h / 60 °C

5: triethylamine; dmap / dichloromethane / 20 °C / Cooling with ice

With dmap; thionyl chloride; sulfuric acid; water; potassium carbonate; triethylamine; sodium hydroxide; In methanol; dichloromethane; toluene; acetonitrile;
DOI:10.1007/s00044-012-0380-8

Reference yield:

: 119-36-8,8024-54-2
methyl salicylate

: 1415750-46-7
2-((6-chloropyridin-3-yl)methoxy)-N-(3,5-dichloro-4-(1,1,2,2-tetrafluoroethoxy)phenyl)benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetonitrile

2: water; sodium hydroxide / methanol

3: thionyl chloride / toluene / 2 h / 60 °C

4: triethylamine; dmap / dichloromethane / 20 °C / Cooling with ice

With dmap; thionyl chloride; water; potassium carbonate; triethylamine; sodium hydroxide; In methanol; dichloromethane; toluene; acetonitrile;
DOI:10.1007/s00044-012-0380-8