3-{3-[4-(4-chloro-phenoxy)-phenylsulfanyl]-2-oxo-propyl}-1,5,5-trimethyl-imidazolidine-2,4-dione

Base Information

Chemical Name:3-{3-[4-(4-chloro-phenoxy)-phenylsulfanyl]-2-oxo-propyl}-1,5,5-trimethyl-imidazolidine-2,4-dione
CAS No.:1026425-51-3
Molecular Formula:C₂₁H₂₁ClN₂O₄S
Molecular Weight:432.928
Hs Code.:

Synonyms:3-{3-[4-(4-chloro-phenoxy)-phenylsulfanyl]-2-oxo-propyl}-1,5,5-trimethyl-imidazolidine-2,4-dione

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Chemical Property of 3-{3-[4-(4-chloro-phenoxy)-phenylsulfanyl]-2-oxo-propyl}-1,5,5-trimethyl-imidazolidine-2,4-dione

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Technology Process of 3-{3-[4-(4-chloro-phenoxy)-phenylsulfanyl]-2-oxo-propyl}-1,5,5-trimethyl-imidazolidine-2,4-dione

There total 3 articles about 3-{3-[4-(4-chloro-phenoxy)-phenylsulfanyl]-2-oxo-propyl}-1,5,5-trimethyl-imidazolidine-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59621-76-0
4-(4'-chlorophenoxy)-benzenethiol

: 220615-58-7
3-(3-bromo-2-oxopropyl)-1,5,5-trimethylimidazolidine-2,4-dione

: 1026425-51-3
3-{3-[4-(4-chloro-phenoxy)-phenylsulfanyl]-2-oxo-propyl}-1,5,5-trimethyl-imidazolidine-2,4-dione

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at -5 ℃; for 1h;
DOI:10.1021/jm0103920

Reference yield:

: 101-79-1
4-amino-4'-chlorodiphenyl ether

: 1026425-51-3
3-{3-[4-(4-chloro-phenoxy)-phenylsulfanyl]-2-oxo-propyl}-1,5,5-trimethyl-imidazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: NaNO₂; aq. HCl / 0.5 h / 0 °C

1.2: aq. HCl / 1 h / 70 °C

2.1: KOH / ethanol / 2 h / 80 °C

3.1: K₂CO₃ / dimethylformamide / 1 h / -5 °C

With hydrogenchloride; potassium hydroxide; potassium carbonate; sodium nitrite; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm0103920

Reference yield:

: dithiocarbonic acid S-[4-(4-chloro-phenoxy)-phenyl] ester O-ethyl ester

: 1026425-51-3
3-{3-[4-(4-chloro-phenoxy)-phenylsulfanyl]-2-oxo-propyl}-1,5,5-trimethyl-imidazolidine-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / ethanol / 2 h / 80 °C

2: K₂CO₃ / dimethylformamide / 1 h / -5 °C

With potassium hydroxide; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm0103920