N,N'-(phenylene-1,3-diyldicarbonyl)bis-L-serine dimethyl ester

Base Information

Chemical Name:N,N'-(phenylene-1,3-diyldicarbonyl)bis-L-serine dimethyl ester
CAS No.:916748-31-7
Molecular Formula:C₁₆H₂₀N₂O₈
Molecular Weight:368.343
Hs Code.:

Synonyms:N,N'-(phenylene-1,3-diyldicarbonyl)bis-L-serine dimethyl ester

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Chemical Property of N,N'-(phenylene-1,3-diyldicarbonyl)bis-L-serine dimethyl ester

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Technology Process of N,N'-(phenylene-1,3-diyldicarbonyl)bis-L-serine dimethyl ester

There total 2 articles about N,N'-(phenylene-1,3-diyldicarbonyl)bis-L-serine dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5680-80-8
methyl (2S)-2-amino-3-hydroxypropanoate hydrochloride

: 99-63-8
benzene-1,3-dicarbonyl dichloride

: 916748-31-7
N,N'-(phenylene-1,3-diyldicarbonyl)bis-L-serine dimethyl ester

Guidance literature:: With triethylamine; In chloroform; at 20 ℃; for 24h;
DOI:10.1002/chem.200600099

Reference yield:

: 121-91-5
isophthalic acid

: 916748-31-7
N,N'-(phenylene-1,3-diyldicarbonyl)bis-L-serine dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 21 h / Heating

2: 1.81 g / triethylamine / CHCl₃ / 24 h / 20 °C

With thionyl chloride; triethylamine; In chloroform;
DOI:10.1002/chem.200600099

Reference yield: 84.0%

: 916748-31-7
N,N'-(phenylene-1,3-diyldicarbonyl)bis-L-serine dimethyl ester

: 916748-32-8
(S,S)-2,2'-(1,3-phenylene)bis(4,5-dihydroxooxazole-4-carboxylic acid) dimethyl ester

Guidance literature:: N,N'-(phenylene-1,3-diyldicarbonyl)bis-L-serine dimethyl ester; With diethylamino-sulfur trifluoride; In dichloromethane; at -78 ℃; for 4h;

With potassium carbonate; In chloroform; at -78 - 20 ℃;
DOI:10.1002/chem.200600099