2-allyloxy-3,5-dibromobenzyl chloride

Base Information

Chemical Name:2-allyloxy-3,5-dibromobenzyl chloride
CAS No.:153034-36-7
Molecular Formula:C₁₀H₉Br₂ClO
Molecular Weight:340.442
Hs Code.:

Synonyms:2-allyloxy-3,5-dibromobenzyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-allyloxy-3,5-dibromobenzyl chloride

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Technology Process of 2-allyloxy-3,5-dibromobenzyl chloride

There total 2 articles about 2-allyloxy-3,5-dibromobenzyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 153034-26-5
2-allyloxy-3,5-dibromobenzyl alcohol

: 153034-36-7
2-allyloxy-3,5-dibromobenzyl chloride

Guidance literature:: With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; for 2h; Heating;
DOI:10.1016/S0040-4020(01)88037-6

Reference yield:

: 90-59-5
3,5-Dibromosalicylaldehyde

: 153034-36-7
2-allyloxy-3,5-dibromobenzyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / NaBH₄ / methanol / 2 h / Heating

2: 72 percent / K₂CO₃ / acetonitrile / 1.5 h / Heating

3: 58 percent / oxalyl chloride, DMF / CH₂Cl₂ / 2 h / Heating

With sodium tetrahydroborate; oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)88037-6